cyclohexyl 3,4,6-tri-O-benzyl-β-D-mannopyranoside

Base Information

Chemical Name:cyclohexyl 3,4,6-tri-O-benzyl-β-D-mannopyranoside
CAS No.:244282-24-4
Molecular Formula:C₃₃H₄₀O₆
Molecular Weight:532.677
Hs Code.:

Synonyms:cyclohexyl 3,4,6-tri-O-benzyl-β-D-mannopyranoside

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Chemical Property of cyclohexyl 3,4,6-tri-O-benzyl-β-D-mannopyranoside

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Technology Process of cyclohexyl 3,4,6-tri-O-benzyl-β-D-mannopyranoside

There total 25 articles about cyclohexyl 3,4,6-tri-O-benzyl-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 244282-23-3
(2R,3R,4S,5S,6R)-3,4-Bis-benzyloxy-2-benzyloxymethyl-5-(1-cyclohexyloxy-2-iodo-1-methyl-ethoxy)-6-phenylsulfanyl-tetrahydro-pyran

: 244282-24-4
cyclohexyl 3,4,6-tri-O-benzyl-β-D-mannopyranoside

Guidance literature:: With N-iodo-succinimide; 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; at 0 - 20 ℃; for 18h;
DOI:10.1016/S0040-4020(01)00308-8

Reference yield: 75.0%

: 118243-90-6
3,4,6-tri-O-benzyl-1,2-O-sulfinyl-α-D-glucopyranoside

: 108-93-0
cyclohexanol

: 244282-24-4
cyclohexyl 3,4,6-tri-O-benzyl-β-D-mannopyranoside

Guidance literature:: With 3 Angstroem MS; ytterbium(III) triflate; In toluene; at 80 ℃; for 1.5h;
DOI:10.1016/0040-4039(94)85307-X

Reference yield: 70.0%

: 358351-73-2
2-O-(1-cyclohexyloxy-2-iodopropyl)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl fluoride

: 244282-24-4
cyclohexyl 3,4,6-tri-O-benzyl-β-D-mannopyranoside

Guidance literature:: 2-O-(1-cyclohexyloxy-2-iodopropyl)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl fluoride; With 2,6-di-tert-butyl-4-methylpyridine; silver trifluoromethanesulfonate; tin(ll) chloride; In acetonitrile; at 50 ℃;

With trifluoroacetic acid; In water; for 0.5h;
DOI:10.1007/s007060200020