diphenylmethyl cholate

Base Information

• Chemical Name: diphenylmethyl cholate
• CAS No.: 459869-01-3
• Molecular Formula: C₃₇H₅₀O₅
• Molecular Weight: 574.801
• Mol file: 459869-01-3.mol

Synonyms:diphenylmethyl cholate

Chemical Property of diphenylmethyl cholate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of diphenylmethyl cholate

There total 1 articles about diphenylmethyl cholate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

cholic acid (81-25-4) + diazodiphenylmethane (908093-98-1) → diphenylmethyl cholate (459869-01-3)

Guidance literature:

In methanol; chloroform; at 45 ℃; for 18h;

DOI:10.1021/jm010359d

Reference yield: 25.0%

3,4-O-dimethoxycarbonyl caffeic acid chloride (16180-95-3) + diphenylmethyl cholate (459869-01-3) → diphenylmethyl 3,12-bis(3,4-dimethoxycarbonylcaffeoyl)cholate + diphenylmethyl 3,7-bis(3,4-dimethoxycarbonylcaffeoyl)cholate + diphenylmethyl 3,7,12-tris(3,4-dimethoxycarbonylcaffeoyl)cholate

Guidance literature:

With pyridine; In benzene; for 4h;

DOI:10.1021/jm010359d

Reference yield:

3,4-O-dimethoxycarbonyl caffeic acid chloride (16180-95-3) + diphenylmethyl cholate (459869-01-3) → 3,12-dicaffeoylcholic acid + 3,7-dicaffeoylcholic acid

Guidance literature:

3,4-O-dimethoxycarbonyl caffeic acid chloride; diphenylmethyl cholate; With pyridine; In benzene; for 4h;

In chloroform; for 3.7h; Heating;

In tetrahydrofuran; methanol; at 20 ℃; for 2h; Further stages. Title compound not separated from byproducts.;

DOI:10.1021/jm010359d

upstream raw materials:

cholic acid

diazodiphenylmethane