(C(CH₃)3C₆H₄)4C₂₀H₆N₄NiNO₂NH₂

Base Information

• Chemical Name: (C(CH₃)3C₆H₄)4C₂₀H₆N₄NiNO₂NH₂
• CAS No.: 944133-11-3
• Molecular Formula: C₆₀H₆₀N₆NiO₂
• Molecular Weight: 955.865
• Mol file: 944133-11-3.mol

Synonyms:(C(CH₃)3C₆H₄)4C₂₀H₆N₄NiNO₂NH₂

Chemical Property of (C(CH₃)3C₆H₄)4C₂₀H₆N₄NiNO₂NH₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (C(CH₃)3C₆H₄)4C₂₀H₆N₄NiNO₂NH₂

There total 1 articles about (C(CH₃)3C₆H₄)4C₂₀H₆N₄NiNO₂NH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

4-amino-1,2,4-triazole (584-13-4) + (C(CH3)3C6H4)4C20H7N4NiNO2 (944133-10-2) → (C(CH3)3C6H4)4C20H6N4NiNO2NH2 (944133-11-3)

Guidance literature:

With NaOH; In ethanol; toluene; Ni complex refluxed with 4-amino-4H-1,2,4-triazole in toluene/EtOH for 1h in the presence of NaOH;

DOI:10.1039/b704681b

Reference yield:

(C(CH3)3C6H4)4C20H6N4NiNO2NH2 (944133-11-3) → (C(CH3)3C6H4)4C20H6N4Ni(NH2)2

Guidance literature:

With sodium tetrahydroborate; palladium 10% on activated carbon; In methanol; dichloromethane; at 25 ℃; for 1h; Inert atmosphere;

DOI:10.1039/c2cc17951b

Reference yield:

sodium tetrahydroborate (16940-66-2) + formic acid (64-18-6) + (C(CH3)3C6H4)4C20H6N4NiNO2NH2 (944133-11-3) → (C(CH3)3C6H4)4C20H6N4NiCHN2H (944133-08-8) + (C(CH3)3C6H4)4C20H6N4NiNH2NHCOH (944133-12-4) + (C(CH3)3C6H4)4C20H6N4Ni(NHCOH)2 (944133-13-5)

Guidance literature:

With Pd/C; In methanol; dichloromethane; toluene; Ni complex reacted with NaBH4 in CH2Cl2/CH3OH in the presence of Pd/C at25°C for 1 h, treated with formic acid in toluene (1:1), refluxe d for 10 min at 110°C; chromy.(silica gel);

DOI:10.1039/b704681b

upstream raw materials:

4-amino-1,2,4-triazole

(C(CH₃)3C₆H₄)4C₂₀H₇N₄NiNO₂

Downstream raw materials:

(C(CH₃)3C₆H₄)4C₂₀H₆N₄NiCHN₂H

(C(CH₃)3C₆H₄)4C₂₀H₆N₄NiNH₂NHCOH

(C(CH₃)3C₆H₄)4C₂₀H₆N₄Ni(NHCOH)2

C₆₀H₅₈N₆Ni