(η6-biphenyl)chloro(ethylenediamine)osmium(II) tetrafluoroborate

Base Information

Chemical Name:(η6-biphenyl)chloro(ethylenediamine)osmium(II) tetrafluoroborate
CAS No.:879132-70-4
Molecular Formula:BF₄*C₁₄H₁₈ClN₂Os
Molecular Weight:526.768
Hs Code.:

Synonyms:(η6-biphenyl)chloro(ethylenediamine)osmium(II) tetrafluoroborate

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Chemical Property of (η6-biphenyl)chloro(ethylenediamine)osmium(II) tetrafluoroborate

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Technology Process of (η6-biphenyl)chloro(ethylenediamine)osmium(II) tetrafluoroborate

There total 2 articles about (η6-biphenyl)chloro(ethylenediamine)osmium(II) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: ammonium tetrafluoroborate

: 879132-66-8
bis[dichlorido(η⁶-biphenyl)osmium(II)]

: 107-15-3,85404-18-8
ethylenediamine

: 879132-70-4
(η6-biphenyl)chloro(ethylenediamine)osmium(II) tetrafluoroborate

Guidance literature:: bis[dichlorido(η⁶-biphenyl)osmium(II)]; ethylenediamine; In methanol; for 0.666667h; Heating / reflux;

ammonium tetrafluoroborate; In methanol;

Reference yield: 54.0%

: 13826-83-0
ammonium tetrafluroborate

: 879132-66-8
bis[dichlorido(η⁶-biphenyl)osmium(II)]

: 107-15-3,85404-18-8
ethylenediamine

: 879132-70-4
(η6-biphenyl)chloro(ethylenediamine)osmium(II) tetrafluoroborate

Guidance literature:: In methanol; under Ar; soln. of Os complex in MeOH heated under reflux for 80 min; NH2CH2CH2NH2 added; heated under reflux for 40 min; filtered while hot; NH4BF4 added; stirred; solvent removed on rotary evaporator; Soxlet extd. (CH2Cl2, 5.5 h); solvent vol. reduced; stored at 253 K overnight; filtered; ppt. washed with CH2Cl2 and Et2O; air dried; elem. anal.;
DOI:10.1021/ic062350d

Reference yield:

: 879132-70-4
(η6-biphenyl)chloro(ethylenediamine)osmium(II) tetrafluoroborate

: 7789-20-0
water-d2

: 940302-62-5
[(η6-biphenyl)(ethylenediamine)osmium(II)(D2O)](2+)

Guidance literature:: With AgNO₃; In water-d2; byproducts: AgCl; addn. of silver salt to a soln. of osmium complex in D2O; filtration through glass wool, NMR detection; Kinetics;
DOI:10.1021/ja055886r