1-iodogermatrane

Base Information

• Chemical Name: 1-iodogermatrane
• CAS No.: 70559-36-3
• Molecular Formula: C₆H₁₂GeINO₃
• Molecular Weight: 345.661
• Mol file: 70559-36-3.mol

Synonyms:1-iodogermatrane

Chemical Property of 1-iodogermatrane

Chemical Property:

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Technology Process of 1-iodogermatrane

There total 1 articles about 1-iodogermatrane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

allyl iodid (556-56-9) + germatrane (67453-19-4) → 1-iodogermatrane (70559-36-3) + allylgermatrane (84664-63-1) + tris(2-hydroxyethyl)amine hydroiodide (7601-53-8)

Guidance literature:

In benzene; under dry N2; mixt. boiled for 35 min; cooled; triethanolamine hydriodide isolated; a mixt. pptd. by evapn. of filtrat;e; recrystd. from hexane and allylgermatrane isolated;

upstream raw materials:

allyl iodid

germatrane