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7601-53-8

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7601-53-8 Usage

Chemical Properties

WHITE CRYSTALLINE POWDER

Check Digit Verification of cas no

The CAS Registry Mumber 7601-53-8 includes 7 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 4 digits, 7,6,0 and 1 respectively; the second part has 2 digits, 5 and 3 respectively.
Calculate Digit Verification of CAS Registry Number 7601-53:
(6*7)+(5*6)+(4*0)+(3*1)+(2*5)+(1*3)=88
88 % 10 = 8
So 7601-53-8 is a valid CAS Registry Number.
InChI:InChI=1/C6H15NO3/c8-4-1-7(2-5-9)3-6-10/h8-10H,1-6H2/p+1

7601-53-8SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 17, 2017

Revision Date: Aug 17, 2017

1.Identification

1.1 GHS Product identifier

Product name 2-[bis(2-hydroxyethyl)amino]ethanol,hydroiodide

1.2 Other means of identification

Product number -
Other names TRIETHANOLAMINE HYDROIODIDE

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:7601-53-8 SDS

7601-53-8Synthetic route

1-(iodomethyl)silatrane
52741-69-2

1-(iodomethyl)silatrane

monophenylthiourea
103-85-5

monophenylthiourea

tris(2-hydroxyethyl)amine hydroiodide
7601-53-8

tris(2-hydroxyethyl)amine hydroiodide

Conditions
ConditionsYield
In butan-1-ol for 12h; Heating;87%
C11H18N2O3SSi*HI

C11H18N2O3SSi*HI

triethanolamine
102-71-6

triethanolamine

A

1-phenyl-2-(2,8,9-trioxa-5-aza-1-sila-bicyclo[3.3.3]undec-1-ylmethyl)-isothiourea; hydriodide

1-phenyl-2-(2,8,9-trioxa-5-aza-1-sila-bicyclo[3.3.3]undec-1-ylmethyl)-isothiourea; hydriodide

B

tris(2-hydroxyethyl)amine hydroiodide
7601-53-8

tris(2-hydroxyethyl)amine hydroiodide

Conditions
ConditionsYield
In chloroformA 83%
B n/a
allyl iodid
556-56-9

allyl iodid

germatrane
67453-19-4

germatrane

A

1-iodogermatrane
70559-36-3

1-iodogermatrane

B

allylgermatrane
84664-63-1

allylgermatrane

C

tris(2-hydroxyethyl)amine hydroiodide
7601-53-8

tris(2-hydroxyethyl)amine hydroiodide

Conditions
ConditionsYield
In benzene under dry N2; mixt. boiled for 35 min; cooled; triethanolamine hydriodide isolated; a mixt. pptd. by evapn. of filtrat;e; recrystd. from hexane and allylgermatrane isolated;A n/a
B 13%
C 50%
triethanolamine
102-71-6

triethanolamine

tris(2-hydroxyethyl)amine hydroiodide
7601-53-8

tris(2-hydroxyethyl)amine hydroiodide

Conditions
ConditionsYield
With hydrogen iodide In water pH=~ 7;
With ammonium iodide
1-(chloromethyl)silatrane
42003-39-4

1-(chloromethyl)silatrane

tris(2-hydroxyethyl)amine hydroiodide
7601-53-8

tris(2-hydroxyethyl)amine hydroiodide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 74 percent / NaI / dimethylformamide / 2.5 h / 20 - 140 °C
2: 87 percent / butan-1-ol / 12 h / Heating
View Scheme
tris(2-hydroxyethyl)amine hydroiodide
7601-53-8

tris(2-hydroxyethyl)amine hydroiodide

antimony triiodide
7790-44-5

antimony triiodide

[triethanolammonium]4[Sb4I16]

[triethanolammonium]4[Sb4I16]

Conditions
ConditionsYield
In dimethyl sulfoxide keeping of mixt. of triethanolammonium iodide, antimony iodide and acetone at room temp. for 24 h; filtration, concn., crystn.; elem. anal.;92%
tris(2-hydroxyethyl)amine hydroiodide
7601-53-8

tris(2-hydroxyethyl)amine hydroiodide

bismuth(III) iodide
7787-64-6

bismuth(III) iodide

triethanolammonium bis(μ3-iodo)tetrakis(μ2-iodo)decaiodotetrabismuthate(III)

triethanolammonium bis(μ3-iodo)tetrakis(μ2-iodo)decaiodotetrabismuthate(III)

Conditions
ConditionsYield
In acetone mixt. of equimolar amt. of ammonium salt and BiI3 in acetone was stirredfor 1 h at 20°C; soln. evapd. for 24 h; elem. anal.;91%

7601-53-8Downstream Products

7601-53-8Relevant articles and documents

Tris(2-hydroxyethyl)ammonium salts: 2,8,9-Trihydroprotatranes

Voronkov,Albanov,Aksamentova,Adamovich,Chipanina,Mirskov,Kochina,Vrazhnov,Litvinov

experimental part, p. 2339 - 2346 (2010/05/15)

New method of synthesis of tris(2-hydroxyethyl)ammonium salts, 2,8,9-trihydroprotatranes X-[HN(CH2CH2OH) 3]+, based on the reaction of tris(2-hydroxyethyl)amine (triethanolamine) with ammonium salts NH4X (X = F, Cl, Br, I, NO 3, ClO4) was developed. 1H, 13C, 15N NMR and IR spectra of these protatranes were investigated, as well as those of their analogs with X = RCH2COO (R = H; 2-MeC 6H4O; 2-Me-4ClC6H3O; 2-MeC 6H4S; 4-ClC6H4S; 4-ClC 6H4SO2; 3-IndS; 3-(PhCH2-IndS) prepared from the corresponding acids RCH2COOH and triethanolamine. The parameters of IR and NMR spectra of the studied protatranes were governed by the nature of substituent X, which also determined the character of the intra and intermolecular hydrogen bonds NH...O and OH...O in the protatrane framework.

S-(trimethoxysilylmethyl)- and S-(silatranylmethyl)isothiuronium halides and their N-substituted derivatives

Sorokin,Lopyrev,Chipanina,Sherstyannikova,Voronkov

, p. 551 - 558 (2007/10/03)

Previously unknown S-(trimethoxysilylmethyl)- and S-(silatranylmethyl) isothiuronium halides and their N-substituted derivatives were prepared. According to the IR and UV spectra, these compounds exist in the solid state and in methanol and acetonitrile solutions in the form of two equilibrium salt structures: those with the positively charged nitrogen and carbon atoms, or predominantly in one of these. In solutions of the iodides in highly polar acetonitrile, the first salt structure can occur in an equilibrium with its dissociation products, S-organylisothiourea (or its N-substituted derivative) and hydrogen iodide.

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