dibutyl (2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)phosphate

Base Information

Chemical Name:dibutyl (2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)phosphate
CAS No.:1391099-65-2
Molecular Formula:C₄₁H₅₉O₁₀PSi
Molecular Weight:770.973
Hs Code.:

Synonyms:dibutyl (2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)phosphate

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Chemical Property of dibutyl (2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)phosphate

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Technology Process of dibutyl (2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)phosphate

There total 2 articles about dibutyl (2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1059116-10-7
dibutyl (2-O-benzoyl-3,4-di-O-benzyl-α-D-mannopyranosyl) phosphate

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1391099-65-2
dibutyl (2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)phosphate

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃;
DOI:10.1021/jo301189y

Reference yield:

: C₂₇H₂₆O₆

: 107-66-4
dibutyl phosphate

: 1391099-65-2
dibutyl (2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 20 °C / Molecular sieve

2: pyridine; dmap / dichloromethane / 20 °C

With pyridine; dmap; In dichloromethane;
DOI:10.1021/jo301189y

Reference yield: 88.0%

: 1391099-65-2
dibutyl (2-O-benzoyl-3,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)phosphate

: (+)-3-O-allyl-4,5,6-O-benzyl-1-O-(4-(3,4-dimethoxyphenyl)benzyl)-1D-myo-inositol

: 3-O-allyl-2-O-(2′-O-benzoyl-3′,4′-di-O-benzyl-6′-O-tert-butyldimethylsilyl-α-D-mannopyranosyl)-4,5,6-tri-O-benzyl-1-O-(4-(3,4-dimethoxyphenyl)benzyl)-1D-myo-inositol

Guidance literature:: With t-butyldimethylsiyl triflate; triethylamine; In toluene; at -78 - 20 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1021/jo5019188