10-(2-(benzylamino)ethyl)-8-(cyclopentyloxy)-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione trifluoroacetate

Base Information

Chemical Name:10-(2-(benzylamino)ethyl)-8-(cyclopentyloxy)-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione trifluoroacetate
CAS No.:1207984-84-6
Molecular Formula:C₂HF₃O₂*C₂₅H₂₇N₅O₃
Molecular Weight:559.545
Hs Code.:

Synonyms:10-(2-(benzylamino)ethyl)-8-(cyclopentyloxy)-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione trifluoroacetate

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Chemical Property of 10-(2-(benzylamino)ethyl)-8-(cyclopentyloxy)-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione trifluoroacetate

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Technology Process of 10-(2-(benzylamino)ethyl)-8-(cyclopentyloxy)-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione trifluoroacetate

There total 9 articles about 10-(2-(benzylamino)ethyl)-8-(cyclopentyloxy)-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1207984-88-0
tert-butyl benzyl(2-(8-(cyclopentyloxy)-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

: 76-05-1
trifluoroacetic acid

: 1207984-84-6
10-(2-(benzylamino)ethyl)-8-(cyclopentyloxy)-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione trifluoroacetate

Guidance literature:: tert-butyl benzyl(2-(8-(cyclopentyloxy)-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;

trifluoroacetic acid; In water; acetonitrile;

Reference yield:

: 95-74-9,827571-80-2
3-chloro-p-toluidine

: 1207984-84-6
10-(2-(benzylamino)ethyl)-8-(cyclopentyloxy)-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione trifluoroacetate

Guidance literature:: Multi-step reaction with 11 steps

1.1: dmap; triethylamine / ethyl acetate / 6 h / 0 - 20 °C

2.1: nitric acid; acetic anhydride / acetic acid / 5 h / -10 - 20 °C

3.1: methanol; sodium methylate / 5 h / 20 °C

4.1: ammonium chloride / ethanol / Reflux; Inert atmosphere

5.1: sodium tetrahydroborate / ethanol / 12 h / Reflux

5.2: 0 - 20 °C

6.1: boron trioxide; acetic acid / 14 h / 20 - 70 °C / Inert atmosphere

7.1: sulfuric acid; periodic acid / water / 0 - 20 °C

7.2: pH 3.8 - 3.9

8.1: acetic acid / ethanol / 20 - 40 °C

8.2: 2 h / 20 °C

9.1: triethylamine / methanol / 2 h / 20 °C

10.1: sodium hydride / 2 h / 70 °C

11.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

11.2: SunFire_.(TM). Prep Cl 8 OBD_.(TM).

With hydrogenchloride; methanol; dmap; boron trioxide; sodium tetrahydroborate; sulfuric acid; nitric acid; sodium methylate; acetic anhydride; sodium hydride; ammonium chloride; acetic acid; periodic acid; triethylamine; In 1,4-dioxane; methanol; ethanol; water; acetic acid; ethyl acetate;

Reference yield:

: 101676-75-9
(8-chloro-7-methyl-2,4-dioxo-3,4-dihydro-2H-benzo[g]pteridin-10-yl)-acetaldehyde

: 1207984-84-6
10-(2-(benzylamino)ethyl)-8-(cyclopentyloxy)-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / ethanol / 20 - 40 °C

1.2: 2 h / 20 °C

2.1: triethylamine / methanol / 2 h / 20 °C

3.1: sodium hydride / 2 h / 70 °C

4.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

4.2: SunFire_.(TM). Prep Cl 8 OBD_.(TM).

With hydrogenchloride; sodium hydride; acetic acid; triethylamine; In 1,4-dioxane; methanol; ethanol;