tert-butyl benzyl(2-(8-(cyclopentyloxy)-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

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Chemical Name:tert-butyl benzyl(2-(8-(cyclopentyloxy)-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate
CAS No.:1207984-88-0
Molecular Formula:C₃₀H₃₅N₅O₅
Molecular Weight:545.638
Hs Code.:

Synonyms:tert-butyl benzyl(2-(8-(cyclopentyloxy)-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

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Chemical Property of tert-butyl benzyl(2-(8-(cyclopentyloxy)-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

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Technology Process of tert-butyl benzyl(2-(8-(cyclopentyloxy)-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

There total 9 articles about tert-butyl benzyl(2-(8-(cyclopentyloxy)-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 96-41-3
Cyclopentanol

: 1207984-86-8
tert-butyl benzyl(2-(8-chloro-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

: 1207984-88-0
tert-butyl benzyl(2-(8-(cyclopentyloxy)-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

Guidance literature:: With sodium hydride; at 70 ℃; for 2h;

Reference yield:

: 95-74-9,827571-80-2
3-chloro-p-toluidine

: 1207984-88-0
tert-butyl benzyl(2-(8-(cyclopentyloxy)-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 10 steps

1.1: dmap; triethylamine / ethyl acetate / 6 h / 0 - 20 °C

2.1: nitric acid; acetic anhydride / acetic acid / 5 h / -10 - 20 °C

3.1: methanol; sodium methylate / 5 h / 20 °C

4.1: ammonium chloride / ethanol / Reflux; Inert atmosphere

5.1: sodium tetrahydroborate / ethanol / 12 h / Reflux

5.2: 0 - 20 °C

6.1: boron trioxide; acetic acid / 14 h / 20 - 70 °C / Inert atmosphere

7.1: sulfuric acid; periodic acid / water / 0 - 20 °C

7.2: pH 3.8 - 3.9

8.1: acetic acid / ethanol / 20 - 40 °C

8.2: 2 h / 20 °C

9.1: triethylamine / methanol / 2 h / 20 °C

10.1: sodium hydride / 2 h / 70 °C

With methanol; dmap; boron trioxide; sodium tetrahydroborate; sulfuric acid; nitric acid; sodium methylate; acetic anhydride; sodium hydride; ammonium chloride; acetic acid; periodic acid; triethylamine; In methanol; ethanol; water; acetic acid; ethyl acetate;

Reference yield:

: 7149-78-2
5-chloro-4-methyl-2-nitroacetanilide

: 1207984-88-0
tert-butyl benzyl(2-(8-(cyclopentyloxy)-7-methyl-2,4-dioxo-3,4-dihydrobenzo[g]pteridin-10(2H)-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 8 steps

1.1: methanol; sodium methylate / 5 h / 20 °C

2.1: ammonium chloride / ethanol / Reflux; Inert atmosphere

3.1: sodium tetrahydroborate / ethanol / 12 h / Reflux

3.2: 0 - 20 °C

4.1: boron trioxide; acetic acid / 14 h / 20 - 70 °C / Inert atmosphere

5.1: sulfuric acid; periodic acid / water / 0 - 20 °C

5.2: pH 3.8 - 3.9

6.1: acetic acid / ethanol / 20 - 40 °C

6.2: 2 h / 20 °C

7.1: triethylamine / methanol / 2 h / 20 °C

8.1: sodium hydride / 2 h / 70 °C

With methanol; boron trioxide; sodium tetrahydroborate; sulfuric acid; sodium methylate; sodium hydride; ammonium chloride; acetic acid; periodic acid; triethylamine; In methanol; ethanol; water;