Technology Process of 2-(5-chloro-4-methyl-2-nitrophenylamino)tetrahydropyran-3,4,5-triol
There total 4 articles about 2-(5-chloro-4-methyl-2-nitrophenylamino)tetrahydropyran-3,4,5-triol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonium chloride;
In
ethanol;
Product distribution / selectivity;
Reflux;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: nitric acid; acetic anhydride / acetic acid / 5 h / -10 - 20 °C
2: methanol; sodium methylate / 5 h / 20 °C
3: ammonium chloride / ethanol / Reflux; Inert atmosphere
With
methanol; nitric acid; sodium methylate; acetic anhydride; ammonium chloride;
In
ethanol; acetic acid;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: methanol; sodium methylate / 5 h / 20 °C
2: ammonium chloride / ethanol / Reflux; Inert atmosphere
With
methanol; sodium methylate; ammonium chloride;
In
ethanol;