N¹,S-Dimethylthiobenzohydrazoniumiodid

Base Information

• Chemical Name: N¹,S-Dimethylthiobenzohydrazoniumiodid
• CAS No.: 37067-45-1
• Molecular Formula: C₉H₁₃N₂S*I
• Molecular Weight: 308.186
• Mol file: 37067-45-1.mol

Synonyms:N¹,S-Dimethylthiobenzohydrazoniumiodid

Chemical Property of N¹,S-Dimethylthiobenzohydrazoniumiodid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N¹,S-Dimethylthiobenzohydrazoniumiodid

There total 1 articles about N¹,S-Dimethylthiobenzohydrazoniumiodid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

N-methylbenzothiohydrazide (21048-05-5) + methyl iodide (74-88-4) → N-methyl-N-(α-methylsulfanyl-benzylidene)-hydrazinium; iodide (37067-45-1)

Guidance literature:

In acetonitrile; for 16h; Ambient temperature;

Reference yield: 95.0%

N1,S-Dimethylthiobenzohydrazoniumiodid (37067-45-1) → methylthiol (74-93-1) + N2-Methylbenzamidrazoniumiodid (83274-32-2)

Guidance literature:

With ammonium hydroxide; In methanol; for 24h; Ambient temperature;

Reference yield: 90.0%

N1,S-Dimethylthiobenzohydrazoniumiodid (37067-45-1) → methylthiol (74-93-1) + N1-Methylbenzamidrazoniumiodid

Guidance literature:

With ammonia; In dichloromethane;

upstream raw materials:

N-methylbenzothiohydrazide

methyl iodide

Downstream raw materials:

N'-[1-(N-Methyl-hydrazino)-1-phenyl-meth-(Z)-ylidene]-hydrazinecarboxylic acid tert-butyl ester

1-Methyl-3,6-diphenyl-1,4-dihydro-1,2,4,5-tetrazin

1-(1,3-Dimethyl-6-phenyl-1,2,3,4-tetrahydro-[1,2,4,5]tetrazin-3-yl)-propan-2-one

1-(1,3-Dimethyl-6-phenyl-1,2,3,4-tetrahydro-[1,2,4,5]tetrazin-3-yl)-ethanone