C₄₄H₄₈O₉

Base Information

Chemical Name:C₄₄H₄₈O₉
CAS No.:123358-24-7
Molecular Formula:C₄₄H₄₈O₉
Molecular Weight:720.86
Hs Code.:

C<sub>44</sub>H<sub>48</sub>O<sub>9</sub>

Synonyms:C₄₄H₄₈O₉

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₄H₄₈O₉

Chemical Property:

Purity/Quality:

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Technology Process of C₄₄H₄₈O₉

There total 21 articles about C₄₄H₄₈O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77573-38-7
C₂₇H₃₈O₈

: 123358-24-7
C₄₄H₄₈O₉

Guidance literature:: Multi-step reaction with 8 steps

1: MnO₂ / CH₂Cl₂

2: H₂ / Pt/C / ethyl acetate / 760 Torr

3: 1.) ArSeCN, (n-Bu)3P, 2.) m-CPBA / 1.) THF, room temp., 2.) CH₂Cl₂, -78 deg C

4: KCN / methanol

5: DMAP / CH₂Cl₂

6: 1.) DIBAH, 2.) DMAP / 1.) toluene, 2.) pyridine, CH₂Cl₂

7: 50 percent / SeO₂, t-BuOOH / CH₂Cl₂ / 0 °C

8: 1.) SOCl₂, propylene oxide, 2.) KOBz, DMAP / 1.) Et₂O, 2.) CH₃CN

With tert.-butylhydroperoxide; dmap; potassium cyanide; manganese(IV) oxide; selenium(IV) oxide; thionyl chloride; tributylphosphine; hydrogen; Potassium benzoate; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; methyloxirane; platinum on activated charcoal; In methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja00206a050

Reference yield:

: 123358-28-1
C₂₇H₃₆O₈

: 123358-24-7
C₄₄H₄₈O₉

Guidance literature:: Multi-step reaction with 7 steps

1: H₂ / Pt/C / ethyl acetate / 760 Torr

2: 1.) ArSeCN, (n-Bu)3P, 2.) m-CPBA / 1.) THF, room temp., 2.) CH₂Cl₂, -78 deg C

3: KCN / methanol

4: DMAP / CH₂Cl₂

5: 1.) DIBAH, 2.) DMAP / 1.) toluene, 2.) pyridine, CH₂Cl₂

6: 50 percent / SeO₂, t-BuOOH / CH₂Cl₂ / 0 °C

7: 1.) SOCl₂, propylene oxide, 2.) KOBz, DMAP / 1.) Et₂O, 2.) CH₃CN

With tert.-butylhydroperoxide; dmap; potassium cyanide; selenium(IV) oxide; thionyl chloride; tributylphosphine; hydrogen; Potassium benzoate; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; methyloxirane; platinum on activated charcoal; In methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja00206a050

Reference yield:

: 77646-25-4
Acetic acid (1aS,1bR,4aS,5R,7aR,7bR,8S,9S,9aR)-9-acetoxy-3-acetoxymethyl-4a,5,7b-trihydroxy-1,1,6,8-tetramethyl-1,1a,1b,4,4a,5,7a,7b,8,9-decahydro-cyclopropa[3,4]benzo[1,2-e]azulen-9a-yl ester

: 123358-24-7
C₄₄H₄₈O₉

Guidance literature:: Multi-step reaction with 10 steps

1: 1.) (n-Bu)4NF, 2.) PPTS / 1.) THF, 2.) CH₂Cl₂

2: HClO₄ / methanol

3: MnO₂ / CH₂Cl₂

4: H₂ / Pt/C / ethyl acetate / 760 Torr

5: 1.) ArSeCN, (n-Bu)3P, 2.) m-CPBA / 1.) THF, room temp., 2.) CH₂Cl₂, -78 deg C

6: KCN / methanol

7: DMAP / CH₂Cl₂

8: 1.) DIBAH, 2.) DMAP / 1.) toluene, 2.) pyridine, CH₂Cl₂

9: 50 percent / SeO₂, t-BuOOH / CH₂Cl₂ / 0 °C

10: 1.) SOCl₂, propylene oxide, 2.) KOBz, DMAP / 1.) Et₂O, 2.) CH₃CN

With tert.-butylhydroperoxide; dmap; potassium cyanide; manganese(IV) oxide; selenium(IV) oxide; thionyl chloride; perchloric acid; tributylphosphine; tetrabutyl ammonium fluoride; hydrogen; Potassium benzoate; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; methyloxirane; platinum on activated charcoal; In methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja00206a050