trans-C₆H₅OIr(CO)(P(p-tolyl)3)2

Base Information

Chemical Name:trans-C₆H₅OIr(CO)(P(p-tolyl)3)2
CAS No.:115338-92-6
Molecular Formula:C₄₉H₄₇IrO₂P₂
Molecular Weight:922.079
Hs Code.:

trans-C<sub>6</sub>H<sub>5</sub>OIr(CO)(P(p-tolyl)3)2

Synonyms:trans-C₆H₅OIr(CO)(P(p-tolyl)3)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-C₆H₅OIr(CO)(P(p-tolyl)3)2

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Technology Process of trans-C₆H₅OIr(CO)(P(p-tolyl)3)2

There total 1 articles about trans-C₆H₅OIr(CO)(P(p-tolyl)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 28195-56-4
trans-carbonylchloro-bis(tri-(p-tolyl)phosphine)iridium(I)

: 139-02-6
sodium phenoxide

: 115338-92-6
trans-C₆H₅OIr(CO)(P(p-tolyl)3)2

Guidance literature:: In tetrahydrofuran; stirring for 20 h at ambient temp. in a drybox under Ar; removal of solvent, dissoln. in toluene, removal of toluene in vacuo, extn.with cyclohexane, filtn., removal of solvent; elem. anal.;
DOI:10.1021/om00099a007

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 115338-92-6
trans-C₆H₅OIr(CO)(P(p-tolyl)3)2

: 28195-56-4
trans-carbonylchloro-bis(tri-(p-tolyl)phosphine)iridium(I)

: 1529-17-5
phenyltrimethylsilyl ether

Guidance literature:: In benzene-d6; Benzene-d6 and silane are condensed into an NMR tube contg. Ir complex (drybox, Ar). After thawing, product is formed within 10 min.; NMR;
DOI:10.1021/om00099a007

Reference yield:

: 115338-92-6
trans-C₆H₅OIr(CO)(P(p-tolyl)3)2

: 115338-91-5
trans-CH₃OIr(CO)(P(p-tolyl)3)2

Guidance literature:: Multi-step reaction with 2 steps

1: benzene-d6

2: tetrahydrofuran

In tetrahydrofuran; benzene-d6;
DOI:10.1021/om00099a007