Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-9-oxo-nonyl ester

Base Information

Chemical Name:Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-9-oxo-nonyl ester
CAS No.:81199-10-2
Molecular Formula:C₂₀H₃₀O₆
Molecular Weight:366.455
Hs Code.:

Synonyms:Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-9-oxo-nonyl ester

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Chemical Property of Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-9-oxo-nonyl ester

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Technology Process of Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-9-oxo-nonyl ester

There total 3 articles about Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-9-oxo-nonyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30993-88-5
9-acetoxy nonanoic acid

: 81199-10-2
Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-9-oxo-nonyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: PCl₅ / CH₂Cl₂ / 2 h / 25 °C

2: AlCl₃ / 1,2-dichloro-ethane / 5 degC, 2 h; 20 degC, 70 h

With aluminium trichloride; phosphorus pentachloride; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1248/cpb.33.4422

Reference yield:

: 29541-97-7
9-acetoxynonal

: 81199-10-2
Acetic acid 9-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-9-oxo-nonyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / KMnO₄, MgSO₄*7H₂O / acetone / 4 h / Ambient temperature

2: PCl₅ / CH₂Cl₂ / 2 h / 25 °C

3: AlCl₃ / 1,2-dichloro-ethane / 5 degC, 2 h; 20 degC, 70 h

With potassium permanganate; aluminium trichloride; phosphorus pentachloride; magnesium sulfate; In dichloromethane; 1,2-dichloro-ethane; acetone;
DOI:10.1248/cpb.33.4422