7-({[4-(4-methyl-1,4-diazepan-1-yl)phenyl]amino}methyl)-2-naphthonitrile

Base Information

Chemical Name:7-({[4-(4-methyl-1,4-diazepan-1-yl)phenyl]amino}methyl)-2-naphthonitrile
CAS No.:771584-73-7
Molecular Formula:C₂₄H₂₆N₄
Molecular Weight:370.497
Hs Code.:

Synonyms:7-({[4-(4-methyl-1,4-diazepan-1-yl)phenyl]amino}methyl)-2-naphthonitrile

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Chemical Property of 7-({[4-(4-methyl-1,4-diazepan-1-yl)phenyl]amino}methyl)-2-naphthonitrile

Chemical Property:

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Technology Process of 7-({[4-(4-methyl-1,4-diazepan-1-yl)phenyl]amino}methyl)-2-naphthonitrile

There total 4 articles about 7-({[4-(4-methyl-1,4-diazepan-1-yl)phenyl]amino}methyl)-2-naphthonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4318-37-0
1-Methylhomopiperazine

: 771584-73-7
7-({[4-(4-methyl-1,4-diazepan-1-yl)phenyl]amino}methyl)-2-naphthonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / K₂CO₃ / dimethylformamide / 17 h / 100 °C

2: H₂ / Pd/C / ethanol / 2 h / 20 °C

3: AcOH; NaB(OAc)3H / CH₂Cl₂ / 2 h / 20 °C

With hydrogen; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; palladium on activated charcoal; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.07.046

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 771584-73-7
7-({[4-(4-methyl-1,4-diazepan-1-yl)phenyl]amino}methyl)-2-naphthonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / K₂CO₃ / dimethylformamide / 17 h / 100 °C

2: H₂ / Pd/C / ethanol / 2 h / 20 °C

3: AcOH; NaB(OAc)3H / CH₂Cl₂ / 2 h / 20 °C

With hydrogen; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; palladium on activated charcoal; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.07.046

Reference yield:

: 223786-22-9
1-methyl-4-(4-nitro-phenyl)-[1,4]-diazepane

: 771584-73-7
7-({[4-(4-methyl-1,4-diazepan-1-yl)phenyl]amino}methyl)-2-naphthonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / ethanol / 2 h / 20 °C

2: AcOH; NaB(OAc)3H / CH₂Cl₂ / 2 h / 20 °C

With hydrogen; sodium tris(acetoxy)borohydride; acetic acid; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1016/j.bmc.2004.07.046