2-methanesulfonylethyl p-phenyl ether

Base Information

Chemical Name:2-methanesulfonylethyl p-phenyl ether
CAS No.:224784-43-4
Molecular Formula:C₄₀H₅₀O₄S
Molecular Weight:626.901
Hs Code.:

2-methanesulfonylethyl p-<tris(p-tert-butylphenyl)methyl>phenyl ether

Synonyms:2-methanesulfonylethyl p-phenyl ether

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Chemical Property of 2-methanesulfonylethyl p-phenyl ether

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Technology Process of 2-methanesulfonylethyl p-phenyl ether

There total 3 articles about 2-methanesulfonylethyl p-phenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 124-63-0
methanesulfonyl chloride

: 224784-42-3
2-hydroxyethyl p-phenyl ether

: 224784-43-4
2-methanesulfonylethyl p-phenyl ether

Guidance literature:: With triethylamine; In dichloromethane; at -2 ℃; for 3.5h;
DOI:10.1021/ja984051w

Reference yield:

: 143998-20-3
4-[tris-(4-tert-butylphenyl)methyl]phenol

: 224784-43-4
2-methanesulfonylethyl p-phenyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 0.46 g / K₂CO₃ / dimethylformamide / 18 h / 65 °C

2: aq. HCl, EtOH / 16 h / Heating

3: 97 percent / Et₃N / CH₂Cl₂ / 3.5 h / -2 °C

With hydrogenchloride; ethanol; potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja984051w

Reference yield:

: 2-(2-{4-[tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-ethoxy)-tetrahydro-pyran

: 224784-43-4
2-methanesulfonylethyl p-phenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl, EtOH / 16 h / Heating

2: 97 percent / Et₃N / CH₂Cl₂ / 3.5 h / -2 °C

With hydrogenchloride; ethanol; triethylamine; In dichloromethane;
DOI:10.1021/ja984051w