Technology Process of methyl 3-(3-methyl-4-methoxyphenyl)glycidate
There total 1 articles about methyl 3-(3-methyl-4-methoxyphenyl)glycidate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium methylate;
In
methanol;
1) -5 deg C, 2 h, 2) room temperature, 3 h;
DOI:10.1021/jm00129a029
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1) NaOCH3, H2O, 2) AcOH / 1) MeOH, overnight, 2) benzene, H2O, 80 deg C
2: 97 percent / benzene / 2 h / Heating
3: 99 percent / H2 / 5percent Pd-C / acetic acid / 2844.3 Torr / Ambient temperature
4: 81 percent / 5percent aq. KOH / 2 h / Heating
With
potassium hydroxide; water; hydrogen; sodium methylate; acetic acid;
palladium on activated charcoal;
In
acetic acid; benzene;
DOI:10.1021/jm00129a029
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) NaOCH3, H2O, 2) AcOH / 1) MeOH, overnight, 2) benzene, H2O, 80 deg C
2: 97 percent / benzene / 2 h / Heating
3: 99 percent / H2 / 5percent Pd-C / acetic acid / 2844.3 Torr / Ambient temperature
With
water; hydrogen; sodium methylate; acetic acid;
palladium on activated charcoal;
In
acetic acid; benzene;
DOI:10.1021/jm00129a029
