2-(ALLYLOXY)-3-METHOXYBENZENECARBALDEHYDE

Base Information

• Chemical Name: 2-(ALLYLOXY)-3-METHOXYBENZENECARBALDEHYDE
• CAS No.: 23343-06-8
• Molecular Formula: C11H12O3
• Molecular Weight: 192.214
• Hs Code.: 2912499000
• Mol file: 23343-06-8.mol

Synonyms:2-Allyloxy-3-methoxy-benzaldehyde;

Chemical Property of 2-(ALLYLOXY)-3-METHOXYBENZENECARBALDEHYDE

Chemical Property:

• Vapor Pressure: 0.000774mmHg at 25°C
• Refractive Index: 1.537
• Boiling Point: 306.4 °C at 760 mmHg
• Flash Point: 130 °C
• PSA: 35.53000
• Density: 1.084 g/cm³
• LogP: 2.07250

Purity/Quality:

98%min ^*data from raw suppliers

2-(Allyloxy)-3-methoxybenzenecarbaldehyde ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(ALLYLOXY)-3-METHOXYBENZENECARBALDEHYDE

There total 4 articles about 2-(ALLYLOXY)-3-METHOXYBENZENECARBALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-methoxy-2-hydroxybenzaldehyde (148-53-8) + allyl bromide (106-95-6) → 2-allyloxy-3-methoxy-benzaldehyde (23343-06-8)

Guidance literature:

With potassium carbonate; In acetone; at 50 ℃;

DOI:10.1055/s-0035-1560501

Reference yield: 92.0%

2-hydroxy-3-methoxybenzaldehyde sodium salt (78166-97-9) + allyl bromide (106-95-6) → 2-allyloxy-3-methoxy-benzaldehyde (23343-06-8)

Guidance literature:

In N,N-dimethyl-formamide; at 25 ℃; for 12h;

DOI:10.1021/jo00330a045

Reference yield: 68.0%

allyl iodid (556-56-9) + 3-methoxy-2-hydroxybenzaldehyde (148-53-8) → 2-allyloxy-3-methoxy-benzaldehyde (23343-06-8)

Guidance literature:

3-methoxy-2-hydroxybenzaldehyde; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

allyl iodid; In N,N-dimethyl-formamide; for 20h;

DOI:10.1021/ja061392y

upstream raw materials:

3-methoxy-2-hydroxybenzaldehyde

allyl bromide

2-hydroxy-3-methoxybenzaldehyde sodium salt

allyl iodid

Downstream raw materials:

6-allylguaicol

1-<2-Allyloxy-3-methoxy-phenyl>-aethanol

2-Allyloxy-3-methoxy-benzaldehyd-dimethylacetal

ethyl α-azido-2-(allyloxy)-3-methoxy-cinnamate