Technology Process of C20H26O
There total 10 articles about C20H26O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
RuCl2[(S)-(DM-SEGPHOS)][(S)-DAIPEN]; potassium tert-butylate; hydrogen;
In
isopropyl alcohol;
at 25 ℃;
for 40h;
under 5171.62 Torr;
Glovebox;
DOI:10.1021/jo3023928
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Dess-Martin periodane / dichloromethane / 0.75 h / 20 °C
2.1: benzene / Irradiation
3.1: potassium tert-butylate / tetrahydrofuran / 0.75 h / 0 °C
3.2: 2 h / 3 - 20 °C
4.1: RuCl2[(S)-(DM-SEGPHOS)][(S)-DAIPEN]; hydrogen; potassium tert-butylate / isopropyl alcohol / 40 h / 25 °C / 5171.62 Torr / Glovebox
With
RuCl2[(S)-(DM-SEGPHOS)][(S)-DAIPEN]; potassium tert-butylate; hydrogen; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane; isopropyl alcohol; benzene;
1.1: |Dess-Martin Oxidation;
DOI:10.1021/jo3023928
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: benzene / Irradiation
2.1: potassium tert-butylate / tetrahydrofuran / 0.75 h / 0 °C
2.2: 2 h / 3 - 20 °C
3.1: RuCl2[(S)-(DM-SEGPHOS)][(S)-DAIPEN]; hydrogen; potassium tert-butylate / isopropyl alcohol / 40 h / 25 °C / 5171.62 Torr / Glovebox
With
RuCl2[(S)-(DM-SEGPHOS)][(S)-DAIPEN]; potassium tert-butylate; hydrogen;
In
tetrahydrofuran; isopropyl alcohol; benzene;
DOI:10.1021/jo3023928
