Technology Process of C25H39NO3
There total 10 articles about C25H39NO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 20 °C
2: pivaloyl chloride; triethylamine; lithium chloride / tetrahydrofuran / -20 - 0 °C
3: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C
With
sodium chlorite; sodium dihydrogenphosphate; sodium hexamethyldisilazane; pivaloyl chloride; triethylamine; lithium chloride;
In
tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2012.08.112
- Guidance literature:
-
Multi-step reaction with 9 steps
1: dilithium tetrachlorocuprate / diethyl ether / -78 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C
3: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 °C
5: diisobutylaluminium hydride / dichloromethane / -78 °C
6: 10 wt% Pd(OH)2 on carbon; triethylamine / benzene / 20 °C
7: sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 20 °C
8: pivaloyl chloride; triethylamine; lithium chloride / tetrahydrofuran / -20 - 0 °C
9: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C
With
sodium chlorite; sodium dihydrogenphosphate; oxalyl dichloride; dilithium tetrachlorocuprate; 10 wt% Pd(OH)2 on carbon; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; pivaloyl chloride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; lithium chloride;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol; benzene;
1: |Grignard Reaction / 3: |Swern Oxidation / 4: |Wittig Olefination;
DOI:10.1016/j.tetlet.2012.08.112