3-[3-(4-Methoxycarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-propionic acid methyl ester; hydrochloride

Base Information

Chemical Name:3-[3-(4-Methoxycarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-propionic acid methyl ester; hydrochloride
CAS No.:90282-10-3
Molecular Formula:C₂₂H₂₇N₃O₆S*ClH
Molecular Weight:498
Hs Code.:

Synonyms:3-[3-(4-Methoxycarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-propionic acid methyl ester; hydrochloride

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Chemical Property of 3-[3-(4-Methoxycarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-propionic acid methyl ester; hydrochloride

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Technology Process of 3-[3-(4-Methoxycarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-propionic acid methyl ester; hydrochloride

There total 4 articles about 3-[3-(4-Methoxycarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-propionic acid methyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 67-56-1
methanol

: 90282-04-5
N-(N_α-Tosyl-4-cyanphenylalanyl)-β-alanin

: 90282-10-3
3-[3-(4-Methoxycarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-propionic acid methyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; for 24h;

Reference yield:

: 18910-26-4,22888-47-7
2-amino-3-(4-cyano-phenyl)-propionic acid

: 90282-10-3
3-[3-(4-Methoxycarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-propionic acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: KOH

2: 85 percent / SOCl₂ / 1 h / Heating

3: 60 percent / NaOH (1 mol/l) / benzene / 4 h / Ambient temperature

4: 85 percent / HCl / dioxane / 24 h

With hydrogenchloride; potassium hydroxide; sodium hydroxide; thionyl chloride; In 1,4-dioxane; benzene;

Reference yield:

: 52117-01-8
N-acetyl-4-cyano-α-(ethoxycarbonyl)phenylalanine ethyl ester

: 90282-10-3
3-[3-(4-Methoxycarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-propionic acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: HCl, CH₃COOH

2: KOH

3: 85 percent / SOCl₂ / 1 h / Heating

4: 60 percent / NaOH (1 mol/l) / benzene / 4 h / Ambient temperature

5: 85 percent / HCl / dioxane / 24 h

With hydrogenchloride; potassium hydroxide; sodium hydroxide; thionyl chloride; acetic acid; In 1,4-dioxane; benzene;