2-(2-nitrophenyl)-2-((trimethylsilyl)oxy)ethyl 4-methylbenzenesulfonate

Base Information

Chemical Name:2-(2-nitrophenyl)-2-((trimethylsilyl)oxy)ethyl 4-methylbenzenesulfonate
CAS No.:1262031-91-3
Molecular Formula:C₁₈H₂₃NO₆SSi
Molecular Weight:409.535
Hs Code.:

Synonyms:2-(2-nitrophenyl)-2-((trimethylsilyl)oxy)ethyl 4-methylbenzenesulfonate

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Chemical Property of 2-(2-nitrophenyl)-2-((trimethylsilyl)oxy)ethyl 4-methylbenzenesulfonate

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Technology Process of 2-(2-nitrophenyl)-2-((trimethylsilyl)oxy)ethyl 4-methylbenzenesulfonate

There total 1 articles about 2-(2-nitrophenyl)-2-((trimethylsilyl)oxy)ethyl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 75-77-4
chloro-trimethyl-silane

: 1262031-90-2
2-hydroxy-2-(2-nitrophenyl)ethyl 4-methylbenzenesulfonate

: 1262031-91-3
2-(2-nitrophenyl)-2-((trimethylsilyl)oxy)ethyl 4-methylbenzenesulfonate

Guidance literature:: With pyridine; at 20 ℃; for 1h;
DOI:10.1002/anie.201408674

Reference yield: 85.0%

: 1262031-91-3
2-(2-nitrophenyl)-2-((trimethylsilyl)oxy)ethyl 4-methylbenzenesulfonate

: 2-azido-1-(o-nitrophenyl)ethanol

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 80 ℃; for 10h; Inert atmosphere;
DOI:10.1039/c0cc02945a

Reference yield:

: 1262031-91-3
2-(2-nitrophenyl)-2-((trimethylsilyl)oxy)ethyl 4-methylbenzenesulfonate

: C₁₄H₁₃N₅O₇

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 80 °C

2: triethylamine / N,N-dimethyl-formamide

With sodium azide; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/ja504692v