dibutyl 3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-2-O-pivaloyl-β-D-glucopyranoside phosphate

Base Information

Chemical Name:dibutyl 3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-2-O-pivaloyl-β-D-glucopyranoside phosphate
CAS No.:943439-96-1
Molecular Formula:C₄₈H₅₉O₁₂P
Molecular Weight:858.963
Hs Code.:

Synonyms:dibutyl 3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-2-O-pivaloyl-β-D-glucopyranoside phosphate

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Chemical Property of dibutyl 3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-2-O-pivaloyl-β-D-glucopyranoside phosphate

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Technology Process of dibutyl 3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-2-O-pivaloyl-β-D-glucopyranoside phosphate

There total 2 articles about dibutyl 3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-2-O-pivaloyl-β-D-glucopyranoside phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 943837-12-5
dibutyl 3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside phosphate

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 943439-96-1
dibutyl 3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-2-O-pivaloyl-β-D-glucopyranoside phosphate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.1080/07328300701298204

Reference yield:

: 226919-66-0
dibutyl 3,4-di-O-benzyl-2-O-pivaloyl-6-O-triisopropylsilyl-β-D-glucopyranoside phpsphate

: 943439-96-1
dibutyl 3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-2-O-pivaloyl-β-D-glucopyranoside phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / TBAF / tetrahydrofuran / 0.5 h / 20 °C

2: 95 percent / pyridine / CH₂Cl₂ / 0.25 h / 20 °C

With pyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1080/07328300701298204

Reference yield: 99.0%

: 943439-96-1
dibutyl 3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-2-O-pivaloyl-β-D-glucopyranoside phosphate

: 943439-97-2
8,8,9,9,10,10,11,11,12,12,13,13,14,14,15,15,15-heptadecafluoropentadec-4(Z)-en-1-ol

: 943439-99-4
[8,8,9,9,10,10,11,11,12,12,13,13,14,14,15,15,15-heptadecafluoropentadec-4(Z)-en-1-yl] 3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside

Guidance literature:: With piperidine; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 0.00833333h;
DOI:10.1021/ol0705503