2-<2-benzyloxy-2-(4-methoxy-1,2-dihydrobenzocyclobuten-1-yl)ethyl>-1,1:3,3-bisethylenedioxy-2-methylcyclopentane

Base Information

Chemical Name:2-<2-benzyloxy-2-(4-methoxy-1,2-dihydrobenzocyclobuten-1-yl)ethyl>-1,1:3,3-bisethylenedioxy-2-methylcyclopentane
CAS No.:76555-93-6
Molecular Formula:C₂₈H₃₄O₆
Molecular Weight:466.574
Hs Code.:

Synonyms:2-<2-benzyloxy-2-(4-methoxy-1,2-dihydrobenzocyclobuten-1-yl)ethyl>-1,1:3,3-bisethylenedioxy-2-methylcyclopentane

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Chemical Property of 2-<2-benzyloxy-2-(4-methoxy-1,2-dihydrobenzocyclobuten-1-yl)ethyl>-1,1:3,3-bisethylenedioxy-2-methylcyclopentane

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Technology Process of 2-<2-benzyloxy-2-(4-methoxy-1,2-dihydrobenzocyclobuten-1-yl)ethyl>-1,1:3,3-bisethylenedioxy-2-methylcyclopentane

There total 2 articles about 2-<2-benzyloxy-2-(4-methoxy-1,2-dihydrobenzocyclobuten-1-yl)ethyl>-1,1:3,3-bisethylenedioxy-2-methylcyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.1%

: 100-39-0
benzyl bromide

: 76555-94-7
1,1:3,3-bisethylenedioxy-2-<2-hydroxy-2-(4-methoxy-1,2-dihydrobenzocyclobuten-1-yl)ethyl>-2-methylcyclopentane

: 76555-93-6
2-<2-benzyloxy-2-(4-methoxy-1,2-dihydrobenzocyclobuten-1-yl)ethyl>-1,1:3,3-bisethylenedioxy-2-methylcyclopentane

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 60 ℃; for 5h;
DOI:10.1039/P19800002793

Reference yield:

: 70833-75-9
7-[1-hydroxy-2-(6-methyl-1,4,8,11-tetraoxa-dispiro[4.1.4.2]tridec-6-yl)-ethyl]-3-methoxy-bicyclo[4.2.0]octa-1,3,5-triene-7-carbonitrile

: 76555-93-6
2-<2-benzyloxy-2-(4-methoxy-1,2-dihydrobenzocyclobuten-1-yl)ethyl>-1,1:3,3-bisethylenedioxy-2-methylcyclopentane

Guidance literature:: Multi-step reaction with 2 steps

1: 81.2 percent / NaH, liquid NH₃, Na / tetrahydrofuran / 1.) room temperature, 30 min, 2.) - 78 deg C, 3 h

2: 92.1 percent / NaH / tetrahydrofuran / 5 h / 60 °C

With ammonia; sodium; sodium hydride; In tetrahydrofuran;
DOI:10.1039/P19800002793