(E)-5-methoxy-2-nitro-β-morpholinestyrene

Base Information

• Chemical Name: (E)-5-methoxy-2-nitro-β-morpholinestyrene
• CAS No.: 107127-61-7
• Molecular Formula: C₁₃H₁₆N₂O₄
• Molecular Weight: 264.281
• Mol file: 107127-61-7.mol

Synonyms:(E)-5-methoxy-2-nitro-β-morpholinestyrene

Chemical Property of (E)-5-methoxy-2-nitro-β-morpholinestyrene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-5-methoxy-2-nitro-β-morpholinestyrene

There total 1 articles about (E)-5-methoxy-2-nitro-β-morpholinestyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

trimorpholylmethane (22630-09-7) + 5-methoxy-2-nitrotoluene (5367-32-8) → (E)-5-methoxy-2-nitro-β-morpholinestyrene (107127-61-7)

Guidance literature:

at 120 - 130 ℃; for 4h; water pump suction;

Reference yield: 72.0%

(E)-5-methoxy-2-nitro-β-morpholinestyrene (107127-61-7) → 5-methoxylindole (1006-94-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In benzene; at 50 ℃; for 8h; under 4560 Torr;

DOI:10.1515/znb-2004-1010

Reference yield: 43.0%

(E)-5-methoxy-2-nitro-β-morpholinestyrene (107127-61-7) + 2-nitrobenzyl chloride (610-14-0) → (E)-2-(5-Methoxy-2-nitro-phenyl)-3-morpholin-4-yl-1-(2-nitro-phenyl)-propenone (107139-49-1)

Guidance literature:

With triethylamine; In benzene; for 15h; Heating;

upstream raw materials:

trimorpholylmethane

5-methoxy-2-nitrotoluene

Downstream raw materials:

(E)-2-(5-Methoxy-2-nitro-phenyl)-3-morpholin-4-yl-1-(2-nitro-phenyl)-propenone

5-methoxylindole

2-(5-Methoxy-2-nitro-phenyl)-1-oxy-indol-3-one

2-(5-Methoxy-2-nitro-phenyl)-1-(2-nitro-phenyl)-ethanone