2-(4-methoxybenzyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one

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Chemical Name:2-(4-methoxybenzyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one
CAS No.:1456613-96-9
Molecular Formula:C₁₂H₁₁N₅O₂S
Molecular Weight:289.318
Hs Code.:

Synonyms:2-(4-methoxybenzyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one

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Chemical Property of 2-(4-methoxybenzyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one

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Technology Process of 2-(4-methoxybenzyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one

There total 5 articles about 2-(4-methoxybenzyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1456614-18-8
C₁₄H₁₇N₅O₃S

: 1456613-96-9
2-(4-methoxybenzyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one

Guidance literature:: With sodium hydroxide; In ethanol; water; at 100 ℃; for 0.333333h;
DOI:10.1016/j.ejmech.2013.06.051

Reference yield:

: 502546-43-2
C₁₀H₁₂N₄O

: 1456613-96-9
2-(4-methoxybenzyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 5 h / 20 °C

2: sodium hydroxide / ethanol; water / 0.33 h / 100 °C

With sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.06.051

Reference yield:

: C₁₀H₁₄N₄O₂

: 1456613-96-9
2-(4-methoxybenzyl)-5-thioxo-5,6-dihydro-[1,2,4]triazolo[1,5-a][1,3,5]triazin-7(4H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: water / 180 °C / Microwave irradiation

2: N,N-dimethyl-formamide / 5 h / 20 °C

3: sodium hydroxide / ethanol; water / 0.33 h / 100 °C

With sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.06.051