ethyl 3-((4-chlorophenyl)amino)-2-(3,4-difluorophenyl)-3-oxo-2-phenylpropanoate

Base Information

Chemical Name:ethyl 3-((4-chlorophenyl)amino)-2-(3,4-difluorophenyl)-3-oxo-2-phenylpropanoate
CAS No.:1391914-26-3
Molecular Formula:C₂₃H₁₈ClF₂NO₃
Molecular Weight:429.851
Hs Code.:

Synonyms:ethyl 3-((4-chlorophenyl)amino)-2-(3,4-difluorophenyl)-3-oxo-2-phenylpropanoate

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Chemical Property of ethyl 3-((4-chlorophenyl)amino)-2-(3,4-difluorophenyl)-3-oxo-2-phenylpropanoate

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Technology Process of ethyl 3-((4-chlorophenyl)amino)-2-(3,4-difluorophenyl)-3-oxo-2-phenylpropanoate

There total 2 articles about ethyl 3-((4-chlorophenyl)amino)-2-(3,4-difluorophenyl)-3-oxo-2-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1391914-19-4
ethyl 3-((4-chlorophenyl)amino)-3-oxo-2-phenylpropanoate

: 217813-00-8
4,5-di-fluoro-2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 1391914-26-3
ethyl 3-((4-chlorophenyl)amino)-2-(3,4-difluorophenyl)-3-oxo-2-phenylpropanoate

Guidance literature:: With cesium fluoride; In acetonitrile; at 20 ℃; for 5h; chemoselective reaction; Inert atmosphere;
DOI:10.1021/ol301768r

Reference yield:

: 15386-84-2
ethyl 3-(4-chloroanilino)-3-oxopropionate

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 1391914-26-3
ethyl 3-((4-chlorophenyl)amino)-2-(3,4-difluorophenyl)-3-oxo-2-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; cesium fluoride / acetonitrile / 12 h / 20 °C / Inert atmosphere

2: cesium fluoride / acetonitrile / 5 h / 20 °C / Inert atmosphere

With triethylamine; cesium fluoride; In acetonitrile;
DOI:10.1021/ol301768r