1,2,3,4-tetra-O-acetyl-6-O-(1,3,4,6-tetra-O-benzoyl-α-D-fructofuranosyl)-β-D-glucopyranose

Base Information

Chemical Name:1,2,3,4-tetra-O-acetyl-6-O-(1,3,4,6-tetra-O-benzoyl-α-D-fructofuranosyl)-β-D-glucopyranose
CAS No.:80768-04-3
Molecular Formula:C₄₈H₄₆O₁₉
Molecular Weight:926.882
Hs Code.:

Synonyms:1,2,3,4-tetra-O-acetyl-6-O-(1,3,4,6-tetra-O-benzoyl-α-D-fructofuranosyl)-β-D-glucopyranose

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Chemical Property of 1,2,3,4-tetra-O-acetyl-6-O-(1,3,4,6-tetra-O-benzoyl-α-D-fructofuranosyl)-β-D-glucopyranose

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Technology Process of 1,2,3,4-tetra-O-acetyl-6-O-(1,3,4,6-tetra-O-benzoyl-α-D-fructofuranosyl)-β-D-glucopyranose

There total 5 articles about 1,2,3,4-tetra-O-acetyl-6-O-(1,3,4,6-tetra-O-benzoyl-α-D-fructofuranosyl)-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 37074-90-1
1,2,3,4-tetra-O-acetyl-6-O-trityl-β-D-glucopyranose

: 80768-03-2,80928-19-4
1,4,6-tri-O-benzoyl-2,3-O-(α-ethylthiobenzylidene)-β-D-fructofuranose

: 80768-04-3
1,2,3,4-tetra-O-acetyl-6-O-(1,3,4,6-tetra-O-benzoyl-α-D-fructofuranosyl)-β-D-glucopyranose

Guidance literature:: With 2,4,6-trimethyl-pyridine; triphenylmethyl perchlorate; In dichloromethane;
DOI:10.1016/S0008-6215(00)81909-6

Reference yield:

: 10489-79-9
α-D-fructofuranose

: 80768-04-3
1,2,3,4-tetra-O-acetyl-6-O-(1,3,4,6-tetra-O-benzoyl-α-D-fructofuranosyl)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 69 percent / pyridine / 0.25 h

2: 40percent HBr, acetic anhydride / CHCl₃; H₂O; acetic acid / 1.5 h / Ambient temperature

3: 25 percent / 2,4,6-trimethyl-pyridine / acetonitrile / Ambient temperature

4: 82 percent / triphenylmethylium perchlorate, 2,4,6-trimethylpyridine / CH₂Cl₂

With pyridine; 2,4,6-trimethyl-pyridine; hydrogen bromide; triphenylmethyl perchlorate; acetic anhydride; In dichloromethane; chloroform; water; acetic acid; acetonitrile;
DOI:10.1016/S0008-6215(00)81909-6

Reference yield:

: 98-88-4
benzoyl chloride

: 80768-04-3
1,2,3,4-tetra-O-acetyl-6-O-(1,3,4,6-tetra-O-benzoyl-α-D-fructofuranosyl)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 69 percent / pyridine / 0.25 h

2: 40percent HBr, acetic anhydride / CHCl₃; H₂O; acetic acid / 1.5 h / Ambient temperature

3: 25 percent / 2,4,6-trimethyl-pyridine / acetonitrile / Ambient temperature

4: 82 percent / triphenylmethylium perchlorate, 2,4,6-trimethylpyridine / CH₂Cl₂

With pyridine; 2,4,6-trimethyl-pyridine; hydrogen bromide; triphenylmethyl perchlorate; acetic anhydride; In dichloromethane; chloroform; water; acetic acid; acetonitrile;
DOI:10.1016/S0008-6215(00)81909-6