(2S,3S)-2-acetoxy-3-((S)-2-benzyloxycarbonylamino-4-methylvalerylamino)tetrahydrofuran

Base Information

• Chemical Name: (2S,3S)-2-acetoxy-3-((S)-2-benzyloxycarbonylamino-4-methylvalerylamino)tetrahydrofuran
• CAS No.: 167765-43-7
• Molecular Formula: C₂₀H₂₈N₂O₆
• Molecular Weight: 392.452

Synonyms:(2S,3S)-2-acetoxy-3-((S)-2-benzyloxycarbonylamino-4-methylvalerylamino)tetrahydrofuran

Chemical Property of (2S,3S)-2-acetoxy-3-((S)-2-benzyloxycarbonylamino-4-methylvalerylamino)tetrahydrofuran

Chemical Property:

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Technology Process of (2S,3S)-2-acetoxy-3-((S)-2-benzyloxycarbonylamino-4-methylvalerylamino)tetrahydrofuran

There total 1 articles about (2S,3S)-2-acetoxy-3-((S)-2-benzyloxycarbonylamino-4-methylvalerylamino)tetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dmap (1122-58-3) + N2-[(benzyloxy)carbonyl]-N1-[(3S)-2-oxotetrahydrofuran-3-yl]-L-leucinamide (167766-55-4) + ethyl acetate n-hexane → (2S,3S)-2-acetoxy-3-((S)-2-benzyloxycarbonylamino-4-methylvalerylamino)tetrahydrofuran (167765-43-7)

Guidance literature:

With acetic anhydride; diisobutylaluminium hydride; In tetrahydrofuran;

Reference yield:

1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride (WSCD.HCl) + N-benzyloxycarbonyl-(L)-leucine (Cbz-Leu-OH) + (2S,3S)-2-acetoxy-3-((S)-2-benzyloxycarbonylamino-4-methylvalerylamino)tetrahydrofuran (167765-43-7) → (2 S,3S)-2-acetoxy-3-[[N-benzyloxycarbonyl-(L)-leucyl-(L)-leucyl]amino]tetrahydrofuran

Guidance literature:

palladium; In N,N-dimethylformamide (DMF); ethanol;

Reference yield:

(2S,3S)-2-acetoxy-3-((S)-2-benzyloxycarbonylamino-4-methylvalerylamino)tetrahydrofuran (167765-43-7) + ethyl acetate n-hexane + ethyl 2-hydroxyacetate (623-50-7) → ethyl [(3S)-3-[[N-benzyloxycarbonyl-(L)-leucyl]amino]tetrahydrofuran-2-yl]oxyacetate

Guidance literature:

With toluene-4-sulfonic acid; In tetrahydrofuran;

upstream raw materials:

dmap

N₂-[(benzyloxy)carbonyl]-N₁-[(3S)-2-oxotetrahydrofuran-3-yl]-L-leucinamide

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