NC(CH₃)CHN₂CS(CH₃)N₂CHC(CH₃)N₂CS(CH₃)NNi

Base Information

• Chemical Name: NC(CH₃)CHN₂CS(CH₃)N₂CHC(CH₃)N₂CS(CH₃)NNi
• CAS No.: 106256-53-5
• Molecular Formula: C₁₀H₁₄N₈NiS₂
• Molecular Weight: 369.097
• Mol file: 106256-53-5.mol

Synonyms:NC(CH₃)CHN₂CS(CH₃)N₂CHC(CH₃)N₂CS(CH₃)NNi

Chemical Property of NC(CH₃)CHN₂CS(CH₃)N₂CHC(CH₃)N₂CS(CH₃)NNi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of NC(CH₃)CHN₂CS(CH₃)N₂CHC(CH₃)N₂CS(CH₃)NNi

There total 1 articles about NC(CH₃)CHN₂CS(CH₃)N₂CHC(CH₃)N₂CS(CH₃)NNi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

nickel(II) chloride hexahydrate + 1H(+)-S-methylisothiocarbonohydrazidium iodide (37839-01-3,67708-03-6) + 2-oxopropanal (78-98-8) → NCHC(CH3)N2CS(CH3)N2CHC(CH3)N2CS(CH3)NNi (105154-39-0,105154-40-3) + NC(CH3)CHN2CS(CH3)N2C(CH3)CHN2CS(CH3)NNi (105154-39-0,105154-40-3) + NC(CH3)CHN2CS(CH3)N2CHC(CH3)N2CS(CH3)NNi (106256-53-5)

Guidance literature:

With pyridine; In ethanol; water; pyridine and methylglyoxal aq. soln. added to soln. of NiCl2*6H2O and S-methylisothiocarbohydrazide hydroiodide in 85% aq. ethanol; mixt. heated to 70°C for 3 h; cooled; ppt. filtered off; washed (acetone); chromy. (silica gel, chloroform); elem. anal.;

upstream raw materials:

1H(+)-S-methylisothiocarbonohydrazidium iodide

2-oxopropanal