cis-N-methyl-3-(4-isopropoxy-3-methoxyphenyl)-4-carboxy-6,7-dimethoxy-3,4-dihydro-1(2H)-isoquinolone

Base Information

Chemical Name:cis-N-methyl-3-(4-isopropoxy-3-methoxyphenyl)-4-carboxy-6,7-dimethoxy-3,4-dihydro-1(2H)-isoquinolone
CAS No.:96705-58-7
Molecular Formula:C₂₃H₂₇NO₇
Molecular Weight:429.47
Hs Code.:

Synonyms:cis-N-methyl-3-(4-isopropoxy-3-methoxyphenyl)-4-carboxy-6,7-dimethoxy-3,4-dihydro-1(2H)-isoquinolone

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Chemical Property of cis-N-methyl-3-(4-isopropoxy-3-methoxyphenyl)-4-carboxy-6,7-dimethoxy-3,4-dihydro-1(2H)-isoquinolone

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Technology Process of cis-N-methyl-3-(4-isopropoxy-3-methoxyphenyl)-4-carboxy-6,7-dimethoxy-3,4-dihydro-1(2H)-isoquinolone

There total 3 articles about cis-N-methyl-3-(4-isopropoxy-3-methoxyphenyl)-4-carboxy-6,7-dimethoxy-3,4-dihydro-1(2H)-isoquinolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 5653-42-9
3,4-dimethoxyhomophthalic anhydride

: 96705-57-6
4-isopropoxy-3-methoxybenzylidenemethylamine

: 96705-59-8
trans-N-methyl-3-(4-isopropoxy-3-methoxyphenyl)-4-carboxy-6,7-dimethoxy-3,4-dihydro-1(2H)-isoquinolone

: 96705-58-7
cis-N-methyl-3-(4-isopropoxy-3-methoxyphenyl)-4-carboxy-6,7-dimethoxy-3,4-dihydro-1(2H)-isoquinolone

Guidance literature:: In chloroform; for 0.5h; Ambient temperature;
DOI:10.1021/jm00146a010

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 96705-58-7
cis-N-methyl-3-(4-isopropoxy-3-methoxyphenyl)-4-carboxy-6,7-dimethoxy-3,4-dihydro-1(2H)-isoquinolone

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / K₂CO₃ / dimethylformamide / 2.5 h / Heating

2: 80 percent / ethanol; H₂O / 6 h / Ambient temperature

3: 65 percent / CHCl₃ / 0.5 h / Ambient temperature

With potassium carbonate; In ethanol; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00146a010

Reference yield:

: 2538-98-9
4-isopropyloxy-3-methoxybenzaldehyde

: 96705-58-7
cis-N-methyl-3-(4-isopropoxy-3-methoxyphenyl)-4-carboxy-6,7-dimethoxy-3,4-dihydro-1(2H)-isoquinolone

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / ethanol; H₂O / 6 h / Ambient temperature

2: 65 percent / CHCl₃ / 0.5 h / Ambient temperature

In ethanol; chloroform; water;
DOI:10.1021/jm00146a010