1-(2,3,5,6-tetrafluoropyridin-4-yl)-3-benzylimidazolium bromide

Base Information

• Chemical Name: 1-(2,3,5,6-tetrafluoropyridin-4-yl)-3-benzylimidazolium bromide
• CAS No.: 1350571-64-0
• Molecular Formula: Br*C₁₅H₁₀F₄N₃
• Molecular Weight: 388.162
• Mol file: 1350571-64-0.mol

Synonyms:1-(2,3,5,6-tetrafluoropyridin-4-yl)-3-benzylimidazolium bromide

Chemical Property of 1-(2,3,5,6-tetrafluoropyridin-4-yl)-3-benzylimidazolium bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(2,3,5,6-tetrafluoropyridin-4-yl)-3-benzylimidazolium bromide

There total 1 articles about 1-(2,3,5,6-tetrafluoropyridin-4-yl)-3-benzylimidazolium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-(2,3,5,6-tetrafluoropyridyl)imidazole (1507306-29-7) + benzyl bromide (100-39-0) → 1-(2,3,5,6-tetrafluoropyridin-4-yl)-3-benzylimidazolium bromide (1350571-64-0)

Guidance literature:

In dichloromethane; at 20 ℃; for 24h;

DOI:10.1021/acs.cgd.5b01077

Reference yield:

1-(2,3,5,6-tetrafluoropyridin-4-yl)-3-benzylimidazolium bromide (1350571-64-0) + mercury(II) diacetate (1600-27-7) → bis{kC-1-(2,3,5,6-tetrafluoropyridyl)-3-benzylimi-dazolin-2-ylidene}tetrabromodimercury

Guidance literature:

In methanol;

DOI:10.1016/j.jfluchem.2015.07.021

Reference yield:

dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer + 1-(2,3,5,6-tetrafluoropyridin-4-yl)-3-benzylimidazolium bromide (1350571-64-0) + silver(l) oxide (20667-12-3) → [(η5-pentamethylcyclopentadienyl)rhodium(III)dichloride(κC-(4-NC5F4)NC3H2NCH2Ph)] + [(η5-pentamethylcyclopentadienyl)rhodium(III)dichloride(κC-(4-NC5F3(OH-2))NC3H2NCH2Ph)] + [(η5-pentamethylcyclopentadienyl)rhodium(III)(chloride)(bromide)(κC-(4-NC5F3(OH-2))NC3H2NCH2Ph)]

Guidance literature:

In dichloromethane; for 4h; Darkness;

DOI:10.1016/j.ica.2012.09.019

upstream raw materials:

1-(2,3,5,6-tetrafluoropyridyl)imidazole

benzyl bromide