4-{[6-(Methylsulfonyl)pyridin-3-yl]oxy}-2-(tetrahydro-2H-pyran-4-yloxy)aniline

Base Information

Chemical Name:4-{[6-(Methylsulfonyl)pyridin-3-yl]oxy}-2-(tetrahydro-2H-pyran-4-yloxy)aniline
CAS No.:1233541-00-8
Molecular Formula:C₁₇H₂₀N₂O₅S
Molecular Weight:364.422
Hs Code.:

Synonyms:4-{[6-(Methylsulfonyl)pyridin-3-yl]oxy}-2-(tetrahydro-2H-pyran-4-yloxy)aniline

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Chemical Property of 4-{[6-(Methylsulfonyl)pyridin-3-yl]oxy}-2-(tetrahydro-2H-pyran-4-yloxy)aniline

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Technology Process of 4-{[6-(Methylsulfonyl)pyridin-3-yl]oxy}-2-(tetrahydro-2H-pyran-4-yloxy)aniline

There total 4 articles about 4-{[6-(Methylsulfonyl)pyridin-3-yl]oxy}-2-(tetrahydro-2H-pyran-4-yloxy)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1233540-99-2
2-(methylsulfonyl)-5-[4-nitro-3-(tetrahydro-2H-pyran-4-yloxy)phenoxy]pyridine

: 1233541-00-8
4-{[6-(Methylsulfonyl)pyridin-3-yl]oxy}-2-(tetrahydro-2H-pyran-4-yloxy)aniline

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; at 50 ℃; for 6h; under 3750.38 Torr;

Reference yield:

: 446-36-6
5-fluoro-2-nitrophenol

: 1233541-00-8
4-{[6-(Methylsulfonyl)pyridin-3-yl]oxy}-2-(tetrahydro-2H-pyran-4-yloxy)aniline

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 100 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 110 °C

3: hydrogen / palladium 10% on activated carbon / ethanol; tetrahydrofuran / 6 h / 50 °C / 3750.38 Torr

With hydrogen; potassium carbonate; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 134419-59-3
4-oxanyl methanesulfonate

: 1233541-00-8
4-{[6-(Methylsulfonyl)pyridin-3-yl]oxy}-2-(tetrahydro-2H-pyran-4-yloxy)aniline

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 100 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 110 °C

3: hydrogen / palladium 10% on activated carbon / ethanol; tetrahydrofuran / 6 h / 50 °C / 3750.38 Torr

With hydrogen; potassium carbonate; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;