tert-butyl 4-(18-(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridinyl)-4,7,10,13,16-pentaoxaoctadecyl)-2,6-di-tert-butylphenyl carbonate

Base Information

Chemical Name:tert-butyl 4-(18-(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridinyl)-4,7,10,13,16-pentaoxaoctadecyl)-2,6-di-tert-butylphenyl carbonate
CAS No.:272770-45-3
Molecular Formula:C₄₅H₆₇NO₁₀
Molecular Weight:782.028
Hs Code.:

Synonyms:tert-butyl 4-(18-(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridinyl)-4,7,10,13,16-pentaoxaoctadecyl)-2,6-di-tert-butylphenyl carbonate

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Chemical Property of tert-butyl 4-(18-(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridinyl)-4,7,10,13,16-pentaoxaoctadecyl)-2,6-di-tert-butylphenyl carbonate

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Technology Process of tert-butyl 4-(18-(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridinyl)-4,7,10,13,16-pentaoxaoctadecyl)-2,6-di-tert-butylphenyl carbonate

There total 9 articles about tert-butyl 4-(18-(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridinyl)-4,7,10,13,16-pentaoxaoctadecyl)-2,6-di-tert-butylphenyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 272770-44-2
tert-butyl 2,6-di-tert-butyl-4-(18-amino-4,7,10,13,16-pentaoxaoctadecyl)phenyl carbonate

: 272770-45-3
tert-butyl 4-(18-(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridinyl)-4,7,10,13,16-pentaoxaoctadecyl)-2,6-di-tert-butylphenyl carbonate

Guidance literature:

Reference yield:

: 4792-15-8
Pentaethylene glycol

: 272770-45-3
tert-butyl 4-(18-(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridinyl)-4,7,10,13,16-pentaoxaoctadecyl)-2,6-di-tert-butylphenyl carbonate

Guidance literature:: Multi-step reaction with 5 steps

1: 41 percent / NaH / dimethylformamide / 0 - 90 °C

2: Et₃N / CH₂Cl₂

3: NaN₃ / dimethylformamide / 90 °C

4: H₂ / PtO₂ / ethanol / 760 Torr

5: ethanol; H₂O / Heating

With sodium azide; hydrogen; sodium hydride; triethylamine; platinum(IV) oxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00698-4

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 272770-45-3
tert-butyl 4-(18-(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridinyl)-4,7,10,13,16-pentaoxaoctadecyl)-2,6-di-tert-butylphenyl carbonate

Guidance literature:: Multi-step reaction with 6 steps

1: 87 percent / DMAP / heptane

2: 41 percent / NaH / dimethylformamide / 0 - 90 °C

3: Et₃N / CH₂Cl₂

4: NaN₃ / dimethylformamide / 90 °C

5: H₂ / PtO₂ / ethanol / 760 Torr

6: ethanol; H₂O / Heating

With dmap; sodium azide; hydrogen; sodium hydride; triethylamine; platinum(IV) oxide; In ethanol; n-heptane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00698-4