tert-butyl 2,6-di-tert-butyl-4-(18-amino-4,7,10,13,16-pentaoxaoctadecyl)phenyl carbonate

Base Information

Chemical Name:tert-butyl 2,6-di-tert-butyl-4-(18-amino-4,7,10,13,16-pentaoxaoctadecyl)phenyl carbonate
CAS No.:272770-44-2
Molecular Formula:C₃₂H₅₇NO₈
Molecular Weight:583.806
Hs Code.:

Synonyms:tert-butyl 2,6-di-tert-butyl-4-(18-amino-4,7,10,13,16-pentaoxaoctadecyl)phenyl carbonate

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Chemical Property of tert-butyl 2,6-di-tert-butyl-4-(18-amino-4,7,10,13,16-pentaoxaoctadecyl)phenyl carbonate

Chemical Property:

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Technology Process of tert-butyl 2,6-di-tert-butyl-4-(18-amino-4,7,10,13,16-pentaoxaoctadecyl)phenyl carbonate

There total 7 articles about tert-butyl 2,6-di-tert-butyl-4-(18-amino-4,7,10,13,16-pentaoxaoctadecyl)phenyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 272770-43-1
carbonic acid 4-{3-[2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-propyl}-2,6-di-tert-butyl-phenyl ester tert-butyl ester

: 272770-44-2
tert-butyl 2,6-di-tert-butyl-4-(18-amino-4,7,10,13,16-pentaoxaoctadecyl)phenyl carbonate

Guidance literature:: With hydrogen; platinum(IV) oxide; In ethanol; under 760 Torr;
DOI:10.1016/S0960-894X(02)00698-4

Reference yield:

: 4792-15-8
Pentaethylene glycol

: 272770-44-2
tert-butyl 2,6-di-tert-butyl-4-(18-amino-4,7,10,13,16-pentaoxaoctadecyl)phenyl carbonate

Guidance literature:: Multi-step reaction with 4 steps

1: 41 percent / NaH / dimethylformamide / 0 - 90 °C

2: Et₃N / CH₂Cl₂

3: NaN₃ / dimethylformamide / 90 °C

4: H₂ / PtO₂ / ethanol / 760 Torr

With sodium azide; hydrogen; sodium hydride; triethylamine; platinum(IV) oxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00698-4

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 272770-44-2
tert-butyl 2,6-di-tert-butyl-4-(18-amino-4,7,10,13,16-pentaoxaoctadecyl)phenyl carbonate

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / DMAP / heptane

2: 41 percent / NaH / dimethylformamide / 0 - 90 °C

3: Et₃N / CH₂Cl₂

4: NaN₃ / dimethylformamide / 90 °C

5: H₂ / PtO₂ / ethanol / 760 Torr

With dmap; sodium azide; hydrogen; sodium hydride; triethylamine; platinum(IV) oxide; In ethanol; n-heptane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00698-4