[3-tert-butoxycarbonyl amino-5-(3-hydroxy-propyl)-phenyl]-carbamic acid tert-butyl ester

Base Information

Chemical Name:[3-tert-butoxycarbonyl amino-5-(3-hydroxy-propyl)-phenyl]-carbamic acid tert-butyl ester
CAS No.:1413947-98-4
Molecular Formula:C₁₉H₃₀N₂O₅
Molecular Weight:366.458
Hs Code.:

Synonyms:[3-tert-butoxycarbonyl amino-5-(3-hydroxy-propyl)-phenyl]-carbamic acid tert-butyl ester

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Chemical Property of [3-tert-butoxycarbonyl amino-5-(3-hydroxy-propyl)-phenyl]-carbamic acid tert-butyl ester

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Technology Process of [3-tert-butoxycarbonyl amino-5-(3-hydroxy-propyl)-phenyl]-carbamic acid tert-butyl ester

There total 8 articles about [3-tert-butoxycarbonyl amino-5-(3-hydroxy-propyl)-phenyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₃₂N₂O₆

: 1413947-98-4
[3-tert-butoxycarbonyl amino-5-(3-hydroxy-propyl)-phenyl]-carbamic acid tert-butyl ester

Guidance literature:: C₂₁H₃₂N₂O₆; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 5h;

With methanol; In tetrahydrofuran;

Reference yield:

: C₁₉H₂₈N₂O₆

: 1413947-98-4
[3-tert-butoxycarbonyl amino-5-(3-hydroxy-propyl)-phenyl]-carbamic acid tert-butyl ester

Guidance literature:: With dimethylsulfide borane complex; In tetrahydrofuran; at 0 ℃; for 1h; Reflux;

Reference yield:

: 28150-13-2
3,5-diaminobenzyl alcohol

: 1413947-98-4
[3-tert-butoxycarbonyl amino-5-(3-hydroxy-propyl)-phenyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1,4-dioxane / 12 h / 20 °C / Alkaline conditions

2: pyridinium chlorochromate; silica gel / dichloromethane / 3 h / 20 °C

3: piperidine; pyridine / 2 h / Reflux

4: palladium 10% on activated carbon; hydrogen / methanol / 5 h / 2280.15 Torr / Autoclave

5: dimethylsulfide borane complex / tetrahydrofuran / 1 h / 0 °C / Reflux

With piperidine; pyridine; dimethylsulfide borane complex; palladium 10% on activated carbon; hydrogen; silica gel; pyridinium chlorochromate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;