di-tert-butyl 5-(hydroxymethyl)-1,3-phenylene dicarbamate

Base Information

Chemical Name:di-tert-butyl 5-(hydroxymethyl)-1,3-phenylene dicarbamate
CAS No.:207745-86-6
Molecular Formula:C₁₇H₂₆N₂O₅
Molecular Weight:338.404
Hs Code.:

Synonyms:di-tert-butyl 5-(hydroxymethyl)-1,3-phenylene dicarbamate

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Chemical Property of di-tert-butyl 5-(hydroxymethyl)-1,3-phenylene dicarbamate

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Technology Process of di-tert-butyl 5-(hydroxymethyl)-1,3-phenylene dicarbamate

There total 3 articles about di-tert-butyl 5-(hydroxymethyl)-1,3-phenylene dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 28150-13-2
3,5-diaminobenzyl alcohol

: 207745-86-6
di-tert-butyl 5-(hydroxymethyl)-1,3-phenylene dicarbamate

Guidance literature:: In 1,4-dioxane; at 20 ℃; for 12h; Alkaline conditions;

Reference yield:

: 99-34-3
3,5-dinitrobenzoic acid

: 207745-86-6
di-tert-butyl 5-(hydroxymethyl)-1,3-phenylene dicarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylsulfide borane complex / tetrahydrofuran / 12 h / 0 °C / Reflux

2: palladium 10% on activated carbon; hydrogen / methanol / 24 h / 2280.15 Torr / Autoclave

3: 1,4-dioxane / 12 h / 20 °C / Alkaline conditions

With dimethylsulfide borane complex; palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; 1,4-dioxane; methanol;

Reference yield:

: 71022-43-0
3,5-dinitrobenzyl alcohol

: 207745-86-6
di-tert-butyl 5-(hydroxymethyl)-1,3-phenylene dicarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 24 h / 2280.15 Torr / Autoclave

2: 1,4-dioxane / 12 h / 20 °C / Alkaline conditions

With palladium 10% on activated carbon; hydrogen; In 1,4-dioxane; methanol;