2-(2-bromo-4-carboxylic acid methyl ester phenoxy)-1-tert-butyldimethylsiloxyethane

Base Information

Chemical Name:2-(2-bromo-4-carboxylic acid methyl ester phenoxy)-1-tert-butyldimethylsiloxyethane
CAS No.:325147-52-2
Molecular Formula:C₁₆H₂₅BrO₄Si
Molecular Weight:389.362
Hs Code.:

Synonyms:2-(2-bromo-4-carboxylic acid methyl ester phenoxy)-1-tert-butyldimethylsiloxyethane

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Chemical Property of 2-(2-bromo-4-carboxylic acid methyl ester phenoxy)-1-tert-butyldimethylsiloxyethane

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Technology Process of 2-(2-bromo-4-carboxylic acid methyl ester phenoxy)-1-tert-butyldimethylsiloxyethane

There total 3 articles about 2-(2-bromo-4-carboxylic acid methyl ester phenoxy)-1-tert-butyldimethylsiloxyethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 29415-97-2
methyl 3-bromo-4-hydroxybenzoate

: 86864-60-0
2-(tert-butyldimethylsilyloxy)ethyl bromide

: 325147-52-2
2-(2-bromo-4-carboxylic acid methyl ester phenoxy)-1-tert-butyldimethylsiloxyethane

Guidance literature:: With potassium carbonate; potassium iodide; In acetonitrile; at 80 ℃; for 16h;
DOI:10.1021/ja005698v

Reference yield:

: 99-76-3,156291-94-0
methyl 4-hydroxylbenzoate

: 325147-52-2
2-(2-bromo-4-carboxylic acid methyl ester phenoxy)-1-tert-butyldimethylsiloxyethane

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Br₂ / CHCl₃ / 14 h / 20 °C

2: 87 percent / K₂CO₃; KI / acetonitrile / 16 h / 80 °C

With bromine; potassium carbonate; potassium iodide; In chloroform; acetonitrile;
DOI:10.1021/ja005698v

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 325147-52-2
2-(2-bromo-4-carboxylic acid methyl ester phenoxy)-1-tert-butyldimethylsiloxyethane

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Et₃N; DMAP / CH₂Cl₂ / 18.5 h / 20 °C

2: 87 percent / K₂CO₃; KI / acetonitrile / 16 h / 80 °C

With dmap; potassium carbonate; triethylamine; potassium iodide; In dichloromethane; acetonitrile;
DOI:10.1021/ja005698v