(E,Z)-2-benzyloxymethyl-1-bromo-1-bromomethyl-3,3-difluorocyclopropane

Base Information

Chemical Name:(E,Z)-2-benzyloxymethyl-1-bromo-1-bromomethyl-3,3-difluorocyclopropane
CAS No.:381221-86-9
Molecular Formula:C₁₂H₁₂Br₂F₂O
Molecular Weight:370.031
Hs Code.:

Synonyms:(E,Z)-2-benzyloxymethyl-1-bromo-1-bromomethyl-3,3-difluorocyclopropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E,Z)-2-benzyloxymethyl-1-bromo-1-bromomethyl-3,3-difluorocyclopropane

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Technology Process of (E,Z)-2-benzyloxymethyl-1-bromo-1-bromomethyl-3,3-difluorocyclopropane

There total 2 articles about (E,Z)-2-benzyloxymethyl-1-bromo-1-bromomethyl-3,3-difluorocyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.1%

: 196495-45-1
2-benzyloxymethyl-3,3-difluoro-1-methylenecyclopropane

: 381221-86-9
(E,Z)-2-benzyloxymethyl-1-bromo-1-bromomethyl-3,3-difluorocyclopropane

Guidance literature:: With pyridinium hydrobromide perbromide; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1021/jm010191w

Reference yield:

: C₁₈H₁₇F₂NO₄Se

: 381221-86-9
(E,Z)-2-benzyloxymethyl-1-bromo-1-bromomethyl-3,3-difluorocyclopropane

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 48 h / 80 °C

2: 95.1 percent / pyridine hydrobromide perbromide / CH₂Cl₂ / 16 h / 20 °C

With pyridinium hydrobromide perbromide; In dichloromethane; toluene;
DOI:10.1021/jm010191w

Reference yield: 31.2%

: 66224-66-6,66224-67-7,66224-68-8,66224-69-9,134434-48-3,134434-49-4,134454-76-5,134461-75-9
adenine

: 381221-86-9
(E,Z)-2-benzyloxymethyl-1-bromo-1-bromomethyl-3,3-difluorocyclopropane

: 376646-48-9
(Z)-9-{[2-(benzyloxymethyl)-3,3-difluorocyclopropylidene]methyl}adenine

: 376646-49-0
(E)-9-{[2-(benzyloxymethyl)-3,3-difluorocyclopropylidene]methyl}adenine

: 9-{[2-(benzyloxymethyl)-3,3-difluorocyclopropenyl]methyl}adenine

Guidance literature:: adenine; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

(E,Z)-2-benzyloxymethyl-1-bromo-1-bromomethyl-3,3-difluorocyclopropane; In N,N-dimethyl-formamide; at 20 ℃; for 16h; Further stages.;
DOI:10.1021/jm010191w