C₂₀H₃₂O₄Si

Base Information

Chemical Name:C₂₀H₃₂O₄Si
CAS No.:916659-67-1
Molecular Formula:C₂₀H₃₂O₄Si
Molecular Weight:364.557
Hs Code.:

C<sub>20</sub>H<sub>32</sub>O<sub>4</sub>Si

Synonyms:C₂₀H₃₂O₄Si

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Chemical Property of C₂₀H₃₂O₄Si

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Technology Process of C₂₀H₃₂O₄Si

There total 5 articles about C₂₀H₃₂O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 916659-61-5
C₂₀H₃₄O₄Si

: 916659-67-1
C₂₀H₃₂O₄Si

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1055/s-2006-950424

Reference yield:

: 80910-01-6,108836-41-5,134733-19-0,144069-33-0
(S)-2-[(4-methoxybenzyloxy)methyl]oxirane

: 916659-67-1
C₂₀H₃₂O₄Si

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / CuI / tetrahydrofuran / 0.17 h / -20 °C

2: 87 percent / Grubbs II catalyst / CH₂Cl₂ / 3 h / Heating

3: 92 percent / imidazole / CH₂Cl₂ / 20 h / 20 °C

4: 85 percent / DIBAL-H / toluene / 4 h / 0 °C

5: 78 percent / Dess-Martin periodinane / CH₂Cl₂ / 3 h / 20 °C

With 1H-imidazole; copper(l) iodide; diisobutylaluminium hydride; Dess-Martin periodane; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1055/s-2006-950424

Reference yield:

: 725715-24-2
(S)-1-((4-methoxybenzyl)oxy)pent-4-en-2-ol

: 916659-67-1
C₂₀H₃₂O₄Si

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / Grubbs II catalyst / CH₂Cl₂ / 3 h / Heating

2: 92 percent / imidazole / CH₂Cl₂ / 20 h / 20 °C

3: 85 percent / DIBAL-H / toluene / 4 h / 0 °C

4: 78 percent / Dess-Martin periodinane / CH₂Cl₂ / 3 h / 20 °C

With 1H-imidazole; diisobutylaluminium hydride; Dess-Martin periodane; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; toluene;
DOI:10.1055/s-2006-950424