5-[4-(4-isopropyloxyphenylsulfonyl)piperazine-1-yl]-2-(1,3-oxazole-2-yl)phenol

Base Information

Chemical Name:5-[4-(4-isopropyloxyphenylsulfonyl)piperazine-1-yl]-2-(1,3-oxazole-2-yl)phenol
CAS No.:932373-10-9
Molecular Formula:C₂₂H₂₅N₃O₅S
Molecular Weight:443.524
Hs Code.:

Synonyms:5-[4-(4-isopropyloxyphenylsulfonyl)piperazine-1-yl]-2-(1,3-oxazole-2-yl)phenol

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Chemical Property of 5-[4-(4-isopropyloxyphenylsulfonyl)piperazine-1-yl]-2-(1,3-oxazole-2-yl)phenol

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Technology Process of 5-[4-(4-isopropyloxyphenylsulfonyl)piperazine-1-yl]-2-(1,3-oxazole-2-yl)phenol

There total 10 articles about 5-[4-(4-isopropyloxyphenylsulfonyl)piperazine-1-yl]-2-(1,3-oxazole-2-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 932373-09-6
C₂₉H₃₁N₃O₅S

: 932373-10-9
5-[4-(4-isopropyloxyphenylsulfonyl)piperazine-1-yl]-2-(1,3-oxazole-2-yl)phenol

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; methanol; for 2h;

Reference yield: 87.6%

: 932372-87-7
4-(4-isopropyloxyphenylsulfonyl)piperazine

: 5-chloro-2-(1,3-oxazole-2-yl)phenol

: 932373-10-9
5-[4-(4-isopropyloxyphenylsulfonyl)piperazine-1-yl]-2-(1,3-oxazole-2-yl)phenol

Guidance literature:: With palladium diacetate; sodium tert-pentoxide; tri-t-butylphosphonium tetraphenylborate complex; In toluene; at 35 - 110 ℃; for 1.5h;

Reference yield:

: 4-chloro-2-hydroxy-N-(2-oxoethyl)benzamide

: 932373-10-9
5-[4-(4-isopropyloxyphenylsulfonyl)piperazine-1-yl]-2-(1,3-oxazole-2-yl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichlorotriphenylphosphorane / acetonitrile / 2.67 h / 25 °C

1.2: 4.87 h / 25 °C

1.3: 1 h / 60 °C

2.1: acetic acid / water; toluene; methanol / 1.32 h / 60 °C

2.2: 1 h / 60 °C

3.1: sodium tert-pentoxide; tri-t-butylphosphonium tetraphenylborate complex; palladium diacetate / toluene / 1.5 h / 35 - 110 °C

With palladium diacetate; sodium tert-pentoxide; acetic acid; tri-t-butylphosphonium tetraphenylborate complex; dichlorotriphenylphosphorane; In methanol; water; toluene; acetonitrile;