methylenebis-2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)-4,1-phenylene diacetate

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Chemical Name:methylenebis-2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)-4,1-phenylene diacetate
CAS No.:1309660-21-6
Molecular Formula:C₃₇H₃₆N₄O₆
Molecular Weight:632.716
Hs Code.:

Synonyms:methylenebis-2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)-4,1-phenylene diacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methylenebis-2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)-4,1-phenylene diacetate

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Technology Process of methylenebis-2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)-4,1-phenylene diacetate

There total 4 articles about methylenebis-2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)-4,1-phenylene diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1174233-50-1
C₃₃H₂₈O₆

: 64-19-7,77671-22-8
acetic acid

: 1309660-21-6
methylenebis-2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)-4,1-phenylene diacetate

Guidance literature:: With hydrazine hydrate; at 180 ℃; for 0.025h; Microwave irradiation;
DOI:10.1016/j.ejmech.2011.03.028

Reference yield:

: 90-02-8
salicylaldehyde

: 1309660-21-6
methylenebis-2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)-4,1-phenylene diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid

2: potassium hydroxide / ethanol

3: hydrazine hydrate / 0.03 h / 180 °C / Microwave irradiation

With sulfuric acid; hydrazine hydrate; potassium hydroxide; In ethanol;
DOI:10.1016/j.ejmech.2011.03.028

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1309660-21-6
methylenebis-2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)-4,1-phenylene diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol

2: hydrazine hydrate / 0.03 h / 180 °C / Microwave irradiation

With hydrazine hydrate; potassium hydroxide; In ethanol;
DOI:10.1016/j.ejmech.2011.03.028