tert-butyl 4-[2-(1-methyl-1H-imidazole-4-sulfonylamino)-ethylamino]-benzoate

Base Information

Chemical Name:tert-butyl 4-[2-(1-methyl-1H-imidazole-4-sulfonylamino)-ethylamino]-benzoate
CAS No.:1247018-60-5
Molecular Formula:C₁₇H₂₄N₄O₄S
Molecular Weight:380.468
Hs Code.:

Synonyms:tert-butyl 4-[2-(1-methyl-1H-imidazole-4-sulfonylamino)-ethylamino]-benzoate

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Chemical Property of tert-butyl 4-[2-(1-methyl-1H-imidazole-4-sulfonylamino)-ethylamino]-benzoate

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Technology Process of tert-butyl 4-[2-(1-methyl-1H-imidazole-4-sulfonylamino)-ethylamino]-benzoate

There total 1 articles about tert-butyl 4-[2-(1-methyl-1H-imidazole-4-sulfonylamino)-ethylamino]-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 99916-98-0
tert-butyl 4-(2-amino-ethylamino)-benzoate

: 137049-00-4
1-methyl-1H-imidazole-4-sulfonyl chloride

: 1247018-60-5
tert-butyl 4-[2-(1-methyl-1H-imidazole-4-sulfonylamino)-ethylamino]-benzoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm1001748

Reference yield: 92.0%

: 1247018-60-5
tert-butyl 4-[2-(1-methyl-1H-imidazole-4-sulfonylamino)-ethylamino]-benzoate

: 100-39-0
benzyl bromide

: 1247018-61-6
tert-butyl 4-{2-[benzyl-(1-methyl-1H-imidazole-4-sulfonyl)-amino]-ethylamino}-benzoate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 0 - 20 ℃; chemoselective reaction; Inert atmosphere;
DOI:10.1021/jm1001748