(3E)-4-[dimethyl(2-methylprop-2-en-1-yl)silyl]-3-methyl-1-phenylbut-3-en-1-ol

Base Information

Chemical Name:(3E)-4-[dimethyl(2-methylprop-2-en-1-yl)silyl]-3-methyl-1-phenylbut-3-en-1-ol
CAS No.:909556-22-5
Molecular Formula:C₁₇H₂₆OSi
Molecular Weight:274.478
Hs Code.:

Synonyms:(3E)-4-[dimethyl(2-methylprop-2-en-1-yl)silyl]-3-methyl-1-phenylbut-3-en-1-ol

Suppliers and Price of (3E)-4-[dimethyl(2-methylprop-2-en-1-yl)silyl]-3-methyl-1-phenylbut-3-en-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3E)-4-[dimethyl(2-methylprop-2-en-1-yl)silyl]-3-methyl-1-phenylbut-3-en-1-ol

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Technology Process of (3E)-4-[dimethyl(2-methylprop-2-en-1-yl)silyl]-3-methyl-1-phenylbut-3-en-1-ol

There total 1 articles about (3E)-4-[dimethyl(2-methylprop-2-en-1-yl)silyl]-3-methyl-1-phenylbut-3-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 100-52-7
benzaldehyde

: 17906-60-4
dimethyl[bis(2-methylprop-2-en-1-yl)]silane

: 909556-22-5
(3E)-4-[dimethyl(2-methylprop-2-en-1-yl)silyl]-3-methyl-1-phenylbut-3-en-1-ol

Guidance literature:: With n-butyllithium; potassium tert-butylate; zinc(II) chloride; In tetrahydrofuran; diethyl ether; hexane; at -78 ℃; for 0.5h;
DOI:10.1021/ol061288l

Reference yield: 83.0%

: 909556-22-5
(3E)-4-[dimethyl(2-methylprop-2-en-1-yl)silyl]-3-methyl-1-phenylbut-3-en-1-ol

: 13329-40-3
4-Iodoacetophenone

: 1-{4-[(1E)-4-hydroxy-2-methyl-4-phenylbut-1-en-1-yl]phenyl}ethanone

Guidance literature:: (3E)-4-[dimethyl(2-methylprop-2-en-1-yl)silyl]-3-methyl-1-phenylbut-3-en-1-ol; With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; ethanol; tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h;

4-Iodoacetophenone; With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; tetrabutyl ammonium fluoride; In tetrahydrofuran; ethanol; at 20 ℃; for 4h;
DOI:10.1021/ol061288l

Reference yield: 82.0%

: 909556-22-5
(3E)-4-[dimethyl(2-methylprop-2-en-1-yl)silyl]-3-methyl-1-phenylbut-3-en-1-ol

: 51934-41-9
4-iodobenzoic acid ethyl ester

: ethyl 4-[(1E)-4-hydroxy-2-methyl-4-phenylbut-1-en-1-yl]benzoate

Guidance literature:: (3E)-4-[dimethyl(2-methylprop-2-en-1-yl)silyl]-3-methyl-1-phenylbut-3-en-1-ol; With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; ethanol; tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h;

4-iodobenzoic acid ethyl ester; With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; tetrabutyl ammonium fluoride; In tetrahydrofuran; ethanol; at 20 ℃; for 4h;
DOI:10.1021/ol061288l