tert-butyl-(2R)-2-({(2E)-2-[(5-chloro-2-iodophenyl)imino]ethanoyl}oxy)propanoate

Base Information

Chemical Name:tert-butyl-(2R)-2-({(2E)-2-[(5-chloro-2-iodophenyl)imino]ethanoyl}oxy)propanoate
CAS No.:476689-66-4
Molecular Formula:C₁₅H₁₇ClINO₄
Molecular Weight:437.662
Hs Code.:

Synonyms:tert-butyl-(2R)-2-({(2E)-2-[(5-chloro-2-iodophenyl)imino]ethanoyl}oxy)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl-(2R)-2-({(2E)-2-[(5-chloro-2-iodophenyl)imino]ethanoyl}oxy)propanoate

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Technology Process of tert-butyl-(2R)-2-({(2E)-2-[(5-chloro-2-iodophenyl)imino]ethanoyl}oxy)propanoate

There total 3 articles about tert-butyl-(2R)-2-({(2E)-2-[(5-chloro-2-iodophenyl)imino]ethanoyl}oxy)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 6828-35-9
5-chloro-2-iodoaniline

: 214278-70-3
tert-butyl-(2R)-2-[(oxoacetyl)oxy]propanoate

: 476689-66-4
tert-butyl-(2R)-2-({(2E)-2-[(5-chloro-2-iodophenyl)imino]ethanoyl}oxy)propanoate

Guidance literature:: In toluene; for 2h; Heating;
DOI:10.1021/jo020327d

Reference yield:

: 68166-83-6
D-lactic acid t-butyl ester

: 476689-66-4
tert-butyl-(2R)-2-({(2E)-2-[(5-chloro-2-iodophenyl)imino]ethanoyl}oxy)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / Et₃N; DMAP / CH₂Cl₂ / 3 h / 0 - 20 °C

2: 100 percent / OsO₄; NaIO₄ / tetrahydrofuran; H₂O / 12 h / 20 °C

3: 100 percent / toluene / 2 h / Heating

With dmap; sodium periodate; osmium(VIII) oxide; triethylamine; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1021/jo020327d

Reference yield:

: 214278-69-0
(1R)-2-tert-butoxy-1-methyl-2-oxoethyl acrylate

: 476689-66-4
tert-butyl-(2R)-2-({(2E)-2-[(5-chloro-2-iodophenyl)imino]ethanoyl}oxy)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / OsO₄; NaIO₄ / tetrahydrofuran; H₂O / 12 h / 20 °C

2: 100 percent / toluene / 2 h / Heating

With sodium periodate; osmium(VIII) oxide; In tetrahydrofuran; water; toluene;
DOI:10.1021/jo020327d