Technology Process of methyl 2-(5-oxocyclohex-3-en-1-yl)acetate
There total 3 articles about methyl 2-(5-oxocyclohex-3-en-1-yl)acetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
dimethyl sulfoxide; toluene;
at 55 ℃;
for 16h;
Inert atmosphere;
DOI:10.1002/anie.201901309
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium chloride / dimethyl sulfoxide; water / 16 h / 160 °C / Inert atmosphere
2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; toluene-4-sulfonic acid / dimethyl sulfoxide; toluene / 16 h / 55 °C / Inert atmosphere
With
toluene-4-sulfonic acid; lithium chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
water; dimethyl sulfoxide; toluene;
DOI:10.1002/anie.201901309
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 3CF3O3S(1-)*Zn(3+) / 20 °C / Inert atmosphere
2: lithium chloride / dimethyl sulfoxide; water / 16 h / 160 °C / Inert atmosphere
3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; toluene-4-sulfonic acid / dimethyl sulfoxide; toluene / 16 h / 55 °C / Inert atmosphere
With
3CF3O3S(1-)*Zn(3+); toluene-4-sulfonic acid; lithium chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
water; dimethyl sulfoxide; toluene;
DOI:10.1002/anie.201901309
