4-chloro-3-methylbenzenediazonium tetrafluoroborate

Base Information

• Chemical Name: 4-chloro-3-methylbenzenediazonium tetrafluoroborate
• CAS No.: 1203587-00-1
• Molecular Formula: BF₄*C₇H₆ClN₂
• Molecular Weight: 240.396
• Mol file: 1203587-00-1.mol

Synonyms:4-chloro-3-methylbenzenediazonium tetrafluoroborate

Chemical Property of 4-chloro-3-methylbenzenediazonium tetrafluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-chloro-3-methylbenzenediazonium tetrafluoroborate

There total 1 articles about 4-chloro-3-methylbenzenediazonium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3-methyl-4-chloroaniline (7149-75-9) → 4-chloro-3-methylbenzenediazonium tetrafluoroborate (1203587-00-1)

Guidance literature:

3-methyl-4-chloroaniline; With hydrogenchloride; sodium nitrite; In water; at -5 ℃; for 0.416667h;

With sodium tetrafluoroborate; In water;

Reference yield:

methanol (67-56-1) + 4-chloro-3-methylbenzenediazonium tetrafluoroborate (1203587-00-1) + N-(tert-butoxycarbonyl)-3-pyrroline (73286-70-1) → tert-butyl 4-(4-chloro-3-methylphenyl)-2-methoxypyrrolidine-1-carboxylate (1203587-01-2)

Guidance literature:

palladium diacetate; at 20 ℃; for 1h; Inert atmosphere;

upstream raw materials:

3-methyl-4-chloroaniline

Downstream raw materials:

tert-butyl 4-(4-chloro-3-methylphenyl)-2-methoxypyrrolidine-1-carboxylate

Refernces