6-(4-(10-phenylanthracen-9-yl)phenoxy)hexyl 5-(1,2-dithiolan-3-yl)pentanoate

Base Information

Chemical Name:6-(4-(10-phenylanthracen-9-yl)phenoxy)hexyl 5-(1,2-dithiolan-3-yl)pentanoate
CAS No.:1443425-52-2
Molecular Formula:C₄₀H₄₂O₃S₂
Molecular Weight:634.904
Hs Code.:

Synonyms:6-(4-(10-phenylanthracen-9-yl)phenoxy)hexyl 5-(1,2-dithiolan-3-yl)pentanoate

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Chemical Property of 6-(4-(10-phenylanthracen-9-yl)phenoxy)hexyl 5-(1,2-dithiolan-3-yl)pentanoate

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Technology Process of 6-(4-(10-phenylanthracen-9-yl)phenoxy)hexyl 5-(1,2-dithiolan-3-yl)pentanoate

There total 3 articles about 6-(4-(10-phenylanthracen-9-yl)phenoxy)hexyl 5-(1,2-dithiolan-3-yl)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 192872-07-4
9-(4-((6-bromohexyl)oxy)phenyl)-10-phenylanthracene

: 1077-28-7,62-46-4
Thioctic acid

: 1443425-52-2
6-(4-(10-phenylanthracen-9-yl)phenoxy)hexyl 5-(1,2-dithiolan-3-yl)pentanoate

Guidance literature:: With dibenzo-18-crown-6; potassium carbonate; In dichloromethane; acetone; at 35 ℃; for 48h;
DOI:10.1039/c3cc42217h

Reference yield:

: 23674-20-6
9-bromo-10-phenylanthracene

: 1443425-52-2
6-(4-(10-phenylanthracen-9-yl)phenoxy)hexyl 5-(1,2-dithiolan-3-yl)pentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate monohydrate / toluene; ethanol; water / 7 h / Inert atmosphere; Reflux

2: tetrabutylammomium bromide; potassium carbonate / acetone / 48 h / Reflux; Inert atmosphere

3: potassium carbonate; dibenzo-18-crown-6 / dichloromethane; acetone / 48 h / 35 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dibenzo-18-crown-6; sodium carbonate monohydrate; tetrabutylammomium bromide; potassium carbonate; In ethanol; dichloromethane; water; acetone; toluene;
DOI:10.1039/c3cc42217h

Reference yield:

: 602-55-1
9-phenylanthracene

: 1443425-52-2
6-(4-(10-phenylanthracen-9-yl)phenoxy)hexyl 5-(1,2-dithiolan-3-yl)pentanoate

Guidance literature:: Multi-step reaction with 4 steps

1: bromine / chloroform / 1.42 h / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate monohydrate / toluene; ethanol; water / 7 h / Inert atmosphere; Reflux

3: tetrabutylammomium bromide; potassium carbonate / acetone / 48 h / Reflux; Inert atmosphere

4: potassium carbonate; dibenzo-18-crown-6 / dichloromethane; acetone / 48 h / 35 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dibenzo-18-crown-6; sodium carbonate monohydrate; tetrabutylammomium bromide; bromine; potassium carbonate; In ethanol; dichloromethane; chloroform; water; acetone; toluene;
DOI:10.1039/c3cc42217h