2,3,6-tri-O-benzoyl-4-O-mesyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

Base Information

Chemical Name:2,3,6-tri-O-benzoyl-4-O-mesyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine
CAS No.:294639-15-9
Molecular Formula:C₃₆H₃₇NO₁₄S
Molecular Weight:739.754
Hs Code.:

Synonyms:2,3,6-tri-O-benzoyl-4-O-mesyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

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Chemical Property of 2,3,6-tri-O-benzoyl-4-O-mesyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

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Technology Process of 2,3,6-tri-O-benzoyl-4-O-mesyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

There total 1 articles about 2,3,6-tri-O-benzoyl-4-O-mesyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 124-63-0
methanesulfonyl chloride

: 2-[((2R,3R,4S,5S,6R)-3,4-Bis-benzoyloxy-6-benzoyloxymethyl-2,5-dihydroxy-tetrahydro-pyran-2-ylamino)-methylene]-malonic acid diethyl ester

: 294639-15-9
2,3,6-tri-O-benzoyl-4-O-mesyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

Guidance literature:: With pyridine; at 20 ℃; for 14h;
DOI:10.1016/S0957-4166(00)00212-3

Reference yield: 92.0%

: 294639-15-9
2,3,6-tri-O-benzoyl-4-O-mesyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

: 294639-17-1
4-azido-2,3,6-tri-O-benzoyl-4-deoxy-N-(2,2-diethoxycarbonylvinyl)-β-D-glucopyranoside

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium azide; at 70 ℃; for 12h;
DOI:10.1016/S0957-4166(00)00212-3

Reference yield:

: 294639-15-9
2,3,6-tri-O-benzoyl-4-O-mesyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

: 294639-19-3
4-amino-2,3,6-tri-O-benzoyl-4-deoxy-N-(2,2-diethoxycarbonylvinyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / NaN₃; hexamethylphosphoramide / 12 h / 70 °C

2: H₂ / Pd/C / methanol / 10 h / 20 °C / 760 Torr

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium azide; hydrogen; palladium on activated charcoal; In methanol; 1: Substitution / 2: Catalytic hydrogenation;
DOI:10.1016/S0957-4166(00)00212-3