3-iodo-4-methoxy-5-propoxybenzaldehyde

Base Information

Chemical Name:3-iodo-4-methoxy-5-propoxybenzaldehyde
CAS No.:1373029-76-5
Molecular Formula:C₁₁H₁₃IO₃
Molecular Weight:320.127
Hs Code.:

Synonyms:3-iodo-4-methoxy-5-propoxybenzaldehyde

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Chemical Property of 3-iodo-4-methoxy-5-propoxybenzaldehyde

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Technology Process of 3-iodo-4-methoxy-5-propoxybenzaldehyde

There total 3 articles about 3-iodo-4-methoxy-5-propoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 54246-07-0
3-hydroxy-5-iodo-4-methoxybenzaldehyde

: 107-08-4
1-iodo-propane

: 1373029-76-5
3-iodo-4-methoxy-5-propoxybenzaldehyde

Guidance literature:: 3-hydroxy-5-iodo-4-methoxybenzaldehyde; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 20 ℃; for 0.583333h; Inert atmosphere;

1-iodo-propane; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1080/00304948.2012.643700

Reference yield:

: 54246-05-8
3-iodo-4,5-dihydroxybenzaldehyde

: 1373029-76-5
3-iodo-4-methoxy-5-propoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.83 h / 20 °C / Inert atmosphere

1.2: 5 h / 20 °C / Inert atmosphere

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.58 h / 20 °C / Inert atmosphere

2.2: 0.5 h / 20 °C / Inert atmosphere

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide;
DOI:10.1080/00304948.2012.643700

Reference yield:

: 5438-36-8
5-iodovaniline

: 1373029-76-5
3-iodo-4-methoxy-5-propoxybenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine; aluminum (III) chloride / dichloromethane / 16.33 h / 50 °C / Inert atmosphere; Reflux

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.83 h / 20 °C / Inert atmosphere

2.2: 5 h / 20 °C / Inert atmosphere

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.58 h / 20 °C / Inert atmosphere

3.2: 0.5 h / 20 °C / Inert atmosphere

With pyridine; aluminum (III) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/00304948.2012.643700